Third grade pottery stone, 26 samples

Colors of the milled samples
Chemical compositions
Mineral compositions
Results of TGA & Colors of the powder samples after measuring
Results of TMA & Colors of the sintered samples after measuring

No.NameSampling dateVein or depositMining placeMining companySampling placeGrade or sort
007USG__07SJuly 16, 1980Sarayama V.GohtsuUeda TohsekiUpper level-centerSK26
043USI3_03SMarch 29, 1980Sarayama V.IguchiyamaUeda Tohseki?Third grade
082USS3_06ANovember 15, 1983Sarayama V.TsurugigasakoUeda TohsekiKawanohata mine ?Third grade, not good face, SK27
075USK3_02AMarch 30, 1982Kaigan V.KawanohataUeda TohsekiNorthThird grade, small grain, high SK
088UKH3P06ANovember 15, 1983Kaigan V.KadonosakoUeda TohsekiOutside driftThird grade, FeS(+)
099KKS__12AJune 11, 1981Kaigan V.ShimizuotoshiKiyama TohsekiStock yard, from WashiyamaHigh SK, SK26
131KKN3_04ANovember 15, 1983Kaigan V.NiiyamaKiyama TohsekiOpen cutThird grade, SK26-27
185MKK3_02ADecember 1, 1980Kaigan V.KawanohataMatsuzaki TohsekiStock yardThird grade, small rock
062UMO3_06AJune 11, 1981Murayama V.Odatoko FuruyashikiUeda TohsekiOpen cut/northHigh SK, third grade, SK20-26
106KGG3_02AMarch 26, 1981Murayama V.GosohKiyama TohsekiIncline shaft working faceThird grade, small rock, SK28, kaolin/sericite=1
143KGY3_03SDecember 1, 1980Murayama V.UchiyamaKyoritsu YogyoMiddle working faceThird grade
146KGY3_06SDecember 1, 1980Murayama V.GosohKyoritsu YogyoWest vein working face/lowerThird grade
151KGY3_11ADecember 1, 1980Murayama V.GosohKyoritsu YogyoEast vein working faceIn the middle of third grade and Shima(stripes)
154KGY3_15ADecember 1, 1980Murayama V.UchiyamaKyoritsu YogyoMiddle working face=KGY3_03S ?, Third grade
169NMF__01AMarch 26, 1981Murayama V.FuruyashikiNishizima Tohseki?Third grade, low SK, average SK=SK20
170NMFTH02AMarch 26, 1981Murayama V.FuruyashikiNishizima Tohseki?Third grade, Shima(stripes), SK18 ?
206HTK3_03AJune 11, 1981Tanosako V.KyogamineHarada TohsekiStock yardThird grade, small rock, SK26
180HFI3S10AMarch 26, 1981Fukami V.FukamiHisatsune TohsekiInside drift/left/second working faceThird grade, Shima(stripes), SK28
181HFI3_12AMarch 26, 1981Fukami V.FukamiHisatsune TohsekiDressing plantThird grade, for insulator
196SFD3_03AMarch 26, 1981Fukami V.FukamiShin-ei TohsekiStock yardThird grade, small rock
197SFD3_04AMarch 26, 1981Fukami V.FukamiShin-ei TohsekiStock yardThird grade A
126K_X__01ADecember 1, 1980Uchida D.SarayamaKiyama TohsekiIn the factory/Middle class pottery clay?
209OOY__02AJune 11, 1981Ooyano D.OoyanoNihon TohsekiStock yard beside national roadBad quality
210OOY__03AJune 11, 1981Ooyano D.OoyanoNihon TohsekiStock yard beside national roadBad quality, Shima(stripes)
213OOY__06AJune 11, 1981Ooyano D.OoyanoHashimoto TohsekiLower level/rightGood quality, white rock
217OOY__10AJune 11, 1981Ooyano D.OoyanoHashimoto TohsekiWaste dumpRaw material of Iwao porcelain Co., Ltd., for tile ?

Colors of the milled samples
No.NameXYZWhiteness
(Hunter)
LabWhiteness
(Lab)
007USG__07S70.6470.5362.6253.0783.983.1714.5878.11
043USI3_03S76.1976.6068.0557.6787.522.2315.1780.23
082USS3_06A77.2976.9369.7959.1487.713.8014.2280.82
075USK3_02A72.0671.0857.6048.8184.315.0318.5175.22
088UKH3P06A73.4973.6471.5960.6785.812.6910.6182.08
099KKS__12A77.7477.2077.4865.6687.864.179.2284.20
131KKN3_04A79.4479.1875.2363.7588.983.6412.1683.19
185MKK3_02A71.4770.0754.6746.3383.715.9219.8773.63
062UMO3_06A82.4182.6184.2571.4090.892.798.6687.12
106KGG3_02A74.6074.2769.6959.0686.183.7012.3881.08
143KGY3_03S66.9166.3753.2745.1481.474.0318.2673.67
146KGY3_06S73.2773.0863.3553.6985.493.3915.9078.20
151KGY3_11A62.5261.9345.8838.8878.704.0920.5270.14
154KGY3_15A75.4175.3961.2851.9386.833.0818.9376.73
169NMF__01A80.6381.5076.7765.0690.281.4412.7883.88
170NMFTH02A71.5471.6261.6152.2184.632.7916.0877.58
206HTK3_03A79.2179.9175.2663.7889.391.7312.6683.39
180HFI3S10A79.2579.2371.2760.4089.013.1614.8481.27
181HFI3_12A74.8674.1266.2356.1386.094.5514.6579.29
196SFD3_03A74.0873.3265.2155.2685.634.5814.7978.88
197SFD3_04A75.7675.2366.3856.2586.744.1315.3479.31
126K_X__01A73.4273.9167.9157.5585.971.9913.3580.54
209OOY__02A75.3376.0964.0154.2587.231.5017.5578.24
210OOY__03A71.4371.3855.2246.8084.493.0620.3974.20
213OOY__06A72.0371.9054.8446.4784.793.2421.0173.86
217OOY__10A75.1275.7365.6655.6487.021.7916.1879.18

Chemical compositions (wt%)
No.NameSiO2Al2O3Fe2O3TiO2CaOMgONa2OK2OIg.loss
007USG__07S78.6614.550.720.010.090.130.111.903.42
043USI3_03S80.9513.110.460.010.050.100.102.902.08
082USS3_06A78.9314.450.610.010.060.140.072.832.51
075USK3_02A77.2715.510.660.010.090.130.073.052.77
088UKH3P06A78.3914.860.630.030.060.100.062.203.36
099KKS__12A78.3514.910.710.020.060.100.062.393.19
131KKN3_04A78.8714.830.600.020.030.110.032.123.19
185MKK3_02A78.0014.890.850.020.130.090.062.972.77
062UMO3_06A79.0614.790.330.020.020.050.092.542.89
106KGG3_02A78.4315.010.770.010.060.050.061.743.66
143KGY3_03S78.4314.570.760.020.000.130.072.952.78
146KGY3_06S79.9013.760.560.010.000.130.082.902.48
151KGY3_11A78.9214.240.970.020.020.100.092.652.77
154KGY3_15A77.9315.170.550.020.070.080.092.902.86
169NMF__01A78.3514.600.800.020.050.130.082.852.52
170NMFTH02A78.0514.680.580.020.010.090.123.362.88
206HTK3_03A79.5314.500.350.050.050.120.082.272.85
180HFI3S10A76.7815.770.390.040.070.070.211.884.50
181HFI3_12A77.3714.920.640.040.100.060.342.153.99
196SFD3_03A78.4314.920.560.030.070.100.121.044.33
197SFD3_04A79.4814.540.460.030.060.070.040.604.35
126K_X__01A73.8217.280.710.030.160.150.263.473.62
209OOY__02A76.0515.810.800.080.060.240.063.223.07
210OOY__03A75.1616.370.850.080.350.240.073.303.25
213OOY__06A75.6816.040.900.080.060.270.093.273.03
217OOY__10A75.8716.270.710.080.030.270.063.233.20

Mineral compositions (wt%)
No.NameQuartzSericiteKaolin mineralFeldsparCalciteSiderite
007USG__07S55.5518.7725.150.530.000.00
043USI3_03S62.3626.869.421.360.000.00
082USS3_06A56.7830.3811.930.740.150.02
075USK3_02A54.1031.6212.961.180.000.14
088UKH3P06A59.0519.9520.250.700.000.05
099KKS__12A60.6319.7918.310.960.000.31
131KKN3_04A61.6015.9521.161.090.080.12
185MKK3_02A60.1327.1011.701.000.000.07
062UMO3_06A63.1219.6016.030.940.290.02
106KGG3_02A59.1015.2125.150.500.000.04
143KGY3_03S57.9624.5815.921.500.000.04
146KGY3_06S65.8118.0214.890.800.000.48
151KGY3_11A56.5226.2015.811.350.000.12
154KGY3_15A63.2118.7816.261.030.720.00
169NMF__01A54.0923.4310.5611.860.000.06
170NMFTH02A51.5630.3117.630.500.000.00
206HTK3_03A48.4537.1513.870.530.000.00
180HFI3S10A53.0612.7833.480.500.180.00
181HFI3_12A47.0227.6524.700.610.000.02
196SFD3_03A54.6314.4730.280.500.090.03
197SFD3_04A58.279.1731.770.500.290.00
126K_X__01A47.3632.9915.583.920.000.15
209OOY__02A54.1526.5518.770.500.000.03
210OOY__03A55.4925.1318.430.700.250.00
213OOY__06A54.5332.2312.730.510.000.00
217OOY__10A55.8020.3122.421.250.000.22

Results of TGA and Colors of the Powder Samples after Measuring
The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1,000°C.
LT : Total weight loss, L400 : Weight loss of 400-1,000°C.
No.NameLT
(wt%)
L400
(wt%)
XYZWhiteness
(Hunter)
LabWhiteness
(Lab)
007USG__07S4.083.1962.9359.9654.7846.4277.439.5612.2672.60
043USI3_03S2.451.9471.7569.2962.1752.6983.248.1913.9976.69
082USS3_06A3.202.3168.0865.1059.5650.4780.689.4212.7175.03
075USK3_02A3.562.5462.8858.8647.0539.8776.7212.0417.3468.57
088UKH3P06A3.913.1770.2467.8663.6853.9782.388.0411.8377.30
099KKS__12A3.563.0164.9863.7265.6055.5979.825.617.1577.87
131KKN3_04A3.573.0371.8869.4065.5555.5583.318.2311.6678.04
185MKK3_02A3.232.6058.8454.0541.2234.9373.5214.2018.2264.86
062UMO3_06A3.292.7578.0276.9777.1265.3687.735.219.2983.75
106KGG3_02A4.033.4766.9064.2961.3351.9780.188.6210.7875.85
143KGY3_03S3.312.5759.9055.3743.0136.4574.4113.4717.8266.03
146KGY3_06S2.872.3467.9965.2157.0248.3280.758.9714.6674.19
151KGY3_11A3.192.5755.3850.5434.8829.5671.0914.6420.6761.56
154KGY3_15A3.452.6966.3561.8248.5841.1778.6313.0418.4068.93
169NMF__01A3.472.3477.3475.8167.7357.4087.076.1814.8379.38
170NMFTH02A3.332.7369.9367.5356.1947.6282.188.0916.9874.09
206HTK3_03A3.242.7579.8078.6974.4263.0788.715.3412.3582.43
180HFI3S10A5.044.3374.4472.2162.5352.9984.987.6615.8576.85
181HFI3_12A4.643.7966.0363.2356.2747.6979.529.0713.7173.74
196SFD3_03A4.994.1064.1361.3253.8045.5978.319.1514.0872.57
197SFD3_04A5.064.1667.4664.4554.6446.3180.289.5015.8472.98
126K_X__01A4.363.3569.6067.0760.7351.4781.908.3813.3675.99
209OOY__02A4.082.8769.3766.4552.9244.8581.529.2518.5772.21
210OOY__03A3.853.0962.6358.3844.5737.7776.4112.6018.9067.25
213OOY__06A3.962.8362.0857.8243.2136.6276.0412.6619.5466.59
217OOY__10A3.763.0770.8669.2859.7950.6783.236.3015.6776.20

Results of TMA and Colors of the Sintered Samples after Measuring
The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SM : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK.
No.NameW10
(wt%)
SM
(%)
T0
(°C)
T5
(°C)
TS5
(°C)
TSK
(°C)
SKXYZW
(Hunter)
LabW
(Lab)
007USG__07S47.36.44143814501445159026+57.5158.6663.8254.0876.590.004.2176.21
043USI3_03S48.99.12143914471441158726+62.7964.1570.3159.5880.09-0.234.0279.69
082USS3_06A49.68.17143214391432158126 58.2559.4864.2654.4677.12-0.154.5976.67
075USK3_02A48.66.80140714181412156526-57.0258.4562.3752.8676.45-0.665.1575.89
088UKH3P06A42.86.82145014601458159927-62.0562.8369.1558.6079.271.023.7678.90
099KKS__12A50.26.35145614601453159527-54.8855.5860.8951.6074.550.933.7674.26
131KKN3_04A45.57.30146014671463160227-64.3765.8273.7062.4681.13-0.352.9380.90
185MKK3_02A50.47.45142714351427157726 68.8770.5479.2467.1583.99-0.612.8583.72
062UMO3_06A51.16.39146614821474160927 70.9672.5381.9269.4285.16-0.312.5884.94
106KGG3_02A47.15.87145414631458159927-53.3654.0959.9150.7773.550.803.1873.34
143KGY3_03S49.18.06143614441437158526 54.8256.2260.6551.4074.98-0.714.5374.56
146KGY3_06S55.37.53147114761465160327-55.1156.3962.6153.0675.09-0.413.1374.89
151KGY3_11A50.08.92143314411434158226 50.1751.2053.5645.3971.55-0.075.7170.99
154KGY3_15A50.26.93145614671460160027-65.2766.4372.8061.6981.500.314.1081.05
169NMF__01A48.66.36139414111405155926-71.1372.5880.2167.9785.19-0.063.8184.71
170NMFTH02A50.87.15144114471439158626+57.9859.4764.9755.0677.12-0.754.0376.75
206HTK3_03A48.97.45147114831477161127 71.3573.0382.6170.0185.46-0.522.5185.23
180HFI3S10A42.56.00148514991497162228-65.0766.5874.8163.4081.60-0.452.7681.39
181HFI3_12A43.58.43147514801477161127 50.7151.7255.9147.3871.920.014.2571.60
196SFD3_03A43.15.85148714991497162228-43.0844.1347.1139.9266.43-0.504.4666.13
197SFD3_04A45.75.75157615831579165029 55.6656.8764.4954.6575.41-0.222.0975.32
126K_X__01A41.17.81136513851384154020+62.9964.4867.0656.8380.30-0.506.7079.19
209OOY__02A48.48.21141114211415156726-57.9459.2964.0554.2877.00-0.434.5876.54
210OOY__03A45.76.04143314411437158426 60.2961.7366.1656.0778.57-0.525.0777.97
213OOY__06A51.26.14140514141406156026-56.5957.9461.4652.0876.12-0.505.4175.51
217OOY__10A46.69.69144314521447159226+60.7062.1567.6457.3278.84-0.524.3178.39
Last updated: August 1997