Kaigan Vein, 38 samples
Colors of the milled samples |
Chemical compositions |
Mineral compositions |
Results of TGA & Colors of the powder samples after measuring |
Results of TMA & Colors of the sintered samples after measuring |
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
---|---|---|---|---|---|---|---|
054 | UKMSA01S | March 29, 1980 | Kaigan V. | Michitanosako | Ueda Tohseki | Upper level | Shima (stripes), Aibite (+) |
055 | UKMH_02A | July 16, 1980 | Kaigan V. | Michitanosako | Ueda Tohseki | Stack | Henshoku (discoloration) |
056 | UKMS_03A | July 16, 1980 | Kaigan V. | Michitanosako | Ueda Tohseki | Stack | Shima (stripes) |
074 | USKS401A | March 30, 1982 | Kaigan V. | Kawanohata | Ueda Tohseki | North | Fourth grade, Shima (stripes), SK20 |
075 | USK3_02A | March 30, 1982 | Kaigan V. | Kawanohata | Ueda Tohseki | North | Third grade, small grain, high SK |
076 | USKH403A | March 30, 1982 | Kaigan V. | Kawanohata | Ueda Tohseki | North | Fourth grade, Henshoku (discoloration), SK26 |
084 | UKHT201A | November 15, 1983 | Kaigan V. | Kadonosako | Ueda Tohseki | Inside drift, south end | Low SK, second grade, FeS (+) |
085 | UKHT202A | November 15, 1983 | Kaigan V. | Kadonosako | Ueda Tohseki | Inside drift, south 10m from end | Low SK, second grade, white rock |
086 | UKH_P03A | November 15, 1983 | Kaigan V. | Kadonosako | Ueda Tohseki | Hamabira Masuyuki | Hard rock, SK17, FeS (+) |
087 | UKHXP05A | November 15, 1983 | Kaigan V. | Kadonosako | Ueda Tohseki | Outside drift | FeS (++), can't use |
088 | UKH3P06A | November 15, 1983 | Kaigan V. | Kadonosako | Ueda Tohseki | Outside drift | Third grade, FeS (+) |
091 | KKS__01A | March 29, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | ? | Representative pottery stone |
092 | KKSHP03A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Center | Henshoku (discoloration), FeS (+), Fe2O3 = 1 wt% |
093 | KKSHP04S | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Inside drift/right | Henshoku (discoloration), FeS (+) |
094 | KKSHP05A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Outside stock | Henshoku (discoloration), FeS (+) |
095 | KKSHA06A | March 26, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Shinyama fifth drift | Henshoku (discoloration), SK20-25 |
096 | KKS__07A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | In the factory of acid treatment | Product, SK18 |
097 | KKS__08A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | In the factory of acid treatment | Raw material |
098 | KKS__11A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Inside drift | Good rock, SK20+ |
099 | KKS__12A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Stock yard, from Washiyama | High SK, SK26 |
100 | KKS__13A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Stock yard | Not good rock, black spot, SK26 ? |
101 | KKS1_14A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Seashore | Recovery, first grade |
102 | KKS0_15A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | ?, Niiyana or Gosoh | Special grade |
103 | KKS1_16A | June 11, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | ? | First grade B, small grain? |
104 | KKSTH17A | November 13, 1982 | Kaigan V. | Iwaotoshi | Kiyama Tohseki | Inside drift | Low SK, Henshoku (discoloration), SK17 |
129 | KKNT_02A | November 15, 1983 | Kaigan V. | Iwaotoshi | Kiyama Tohseki | Fifth drift, next Niiyama | Low SK, SK14 |
130 | KKNS_03A | November 15, 1983 | Kaigan V. | Niiyama | Kiyama Tohseki | Open cut | Shima (stripes), raw material for acid treatment |
131 | KKN3_04A | November 15, 1983 | Kaigan V. | Niiyama | Kiyama Tohseki | Open cut | Third grade, SK26-27 |
132 | KKH__01A | November 15, 1983 | Kaigan V. | Hachikubo | Kiyama Tohseki | Front of old drift | Low SK, homogeneous |
133 | KKH__02A | November 15, 1983 | Kaigan V. | Hachikubo | Kiyama Tohseki | ? | Waste rock, raw material for low grade pottery clay ? |
134 | KHDHP01A | November 15, 1983 | Kaigan V. | Tanohira | Kiyama Tohseki | Open cut | FeS (+), Henshoku (discoloration), SK26-27 |
184 | MKK2_01S | December 1, 1980 | Kaigan V. | Kawanohata | Matsuzaki Tohseki | Stock yard | Second grade |
185 | MKK3_02A | December 1, 1980 | Kaigan V. | Kawanohata | Matsuzaki Tohseki | Stock yard | Third grade, small rock |
186 | MKKH_03A | December 1, 1980 | Kaigan V. | Kawanohata | Matsuzaki Tohseki | Stock yard | Henshoku (discoloration) |
200 | HTO__01S | June 11, 1981 | Kaigan V. | Ohsako | Harada Tohseki | Center | Good rock, rough surface, SK18 ? |
201 | HTO4_02A | June 11, 1981 | Kaigan V. | Ohsako | Harada Tohseki | Right wall | Good rock, Fourth grade ? |
202 | HTOTA03A | June 11, 1981 | Kaigan V. | Ohsako | Harada Tohseki | Center/left | Low grade, Albite (+) |
203 | HTOSA04A | June 11, 1981 | Kaigan V. | Ohsako | Harada Tohseki | Center/right | Lowest grade ?, Shima (stripes) & Albite |
Colors of the milled samples | |||||||||
---|---|---|---|---|---|---|---|---|---|
No. | Name | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
054 | UKMSA01S | 61.84 | 60.06 | 43.05 | 36.48 | 77.50 | 6.81 | 21.31 | 68.27 |
055 | UKMH_02A | 82.53 | 83.11 | 88.57 | 75.06 | 91.16 | 2.06 | 6.21 | 89.01 |
056 | UKMS_03A | 71.17 | 70.32 | 54.65 | 46.31 | 83.86 | 4.74 | 20.06 | 73.82 |
074 | USKS401A | 69.39 | 68.09 | 49.97 | 42.35 | 82.52 | 5.70 | 21.86 | 71.44 |
075 | USK3_02A | 72.06 | 71.08 | 57.60 | 48.81 | 84.31 | 5.03 | 18.51 | 75.22 |
076 | USKH403A | 69.93 | 69.27 | 69.34 | 58.76 | 83.23 | 4.33 | 8.86 | 80.54 |
084 | UKHT201A | 81.28 | 82.05 | 85.70 | 72.63 | 90.58 | 1.65 | 7.31 | 87.96 |
085 | UKHT202A | 84.08 | 84.71 | 88.23 | 74.77 | 92.04 | 2.00 | 7.59 | 88.82 |
086 | UKH_P03A | 73.45 | 74.00 | 83.47 | 70.74 | 86.02 | 1.87 | 2.69 | 85.65 |
087 | UKHXP05A | 73.94 | 74.61 | 83.44 | 70.71 | 86.38 | 1.64 | 3.19 | 85.91 |
088 | UKH3P06A | 73.49 | 73.64 | 71.59 | 60.67 | 85.81 | 2.69 | 10.61 | 82.08 |
091 | KKS__01A | 75.58 | 75.37 | 70.45 | 59.70 | 86.82 | 3.47 | 12.66 | 81.40 |
092 | KKSHP03A | 76.95 | 76.46 | 71.21 | 60.35 | 87.44 | 4.06 | 12.92 | 81.53 |
093 | KKSHP04S | 77.96 | 77.81 | 82.57 | 69.97 | 88.21 | 3.39 | 6.25 | 86.23 |
094 | KKSHP05A | 79.42 | 79.39 | 80.67 | 68.36 | 89.10 | 3.18 | 8.69 | 85.70 |
095 | KKSHA06A | 82.95 | 83.24 | 90.12 | 76.37 | 91.24 | 2.63 | 5.30 | 89.43 |
096 | KKS__07A | 85.11 | 85.50 | 92.03 | 77.99 | 92.47 | 2.48 | 5.72 | 90.22 |
097 | KKS__08A | 71.19 | 70.76 | 61.37 | 52.01 | 84.12 | 3.86 | 15.63 | 77.39 |
098 | KKS__11A | 80.41 | 80.17 | 89.09 | 75.50 | 89.54 | 3.61 | 3.68 | 88.34 |
099 | KKS__12A | 77.74 | 77.20 | 77.48 | 65.66 | 87.86 | 4.17 | 9.22 | 84.20 |
100 | KKS__13A | 84.09 | 84.31 | 91.83 | 77.82 | 91.82 | 2.79 | 4.98 | 90.03 |
101 | KKS1_14A | 85.18 | 86.78 | 94.04 | 79.69 | 93.16 | 0.19 | 5.36 | 91.31 |
102 | KKS0_15A | 83.85 | 84.94 | 94.27 | 79.89 | 92.16 | 1.11 | 3.87 | 91.19 |
103 | KKS1_16A | 78.87 | 79.22 | 84.25 | 71.40 | 89.01 | 2.41 | 6.18 | 87.16 |
104 | KKSTH17A | 77.63 | 78.17 | 73.32 | 62.14 | 88.41 | 2.00 | 12.72 | 82.68 |
129 | KKNT_02A | 82.31 | 82.89 | 89.81 | 76.11 | 91.04 | 2.05 | 5.24 | 89.42 |
130 | KKNS_03A | 65.46 | 64.55 | 51.98 | 44.05 | 80.34 | 4.83 | 17.88 | 72.99 |
131 | KKN3_04A | 79.44 | 79.18 | 75.23 | 63.75 | 88.98 | 3.64 | 12.16 | 83.19 |
132 | KKH__01A | 81.40 | 81.74 | 80.09 | 67.87 | 90.41 | 2.49 | 10.76 | 85.37 |
133 | KKH__02A | 71.31 | 70.13 | 55.09 | 46.69 | 83.74 | 5.45 | 19.62 | 73.95 |
134 | KHDHP01A | 78.94 | 79.49 | 78.92 | 66.88 | 89.16 | 2.02 | 9.93 | 85.16 |
184 | MKK2_01S | 81.19 | 81.11 | 84.71 | 71.79 | 90.06 | 3.31 | 7.28 | 87.25 |
185 | MKK3_02A | 71.47 | 70.07 | 54.67 | 46.33 | 83.71 | 5.92 | 19.87 | 73.63 |
186 | MKKH_03A | 72.34 | 71.30 | 61.87 | 52.43 | 84.44 | 5.15 | 15.66 | 77.33 |
200 | HTO__01S | 63.54 | 62.05 | 44.33 | 37.57 | 78.77 | 6.13 | 21.77 | 68.98 |
201 | HTO4_02A | 62.07 | 60.59 | 43.97 | 37.26 | 77.84 | 6.12 | 21.00 | 68.87 |
202 | HTOTA03A | 62.70 | 61.62 | 46.30 | 39.24 | 78.50 | 5.20 | 19.98 | 70.19 |
203 | HTOSA04A | 57.05 | 55.00 | 37.60 | 31.86 | 74.16 | 7.53 | 21.85 | 65.33 |
Chemical compositions (wt%) | ||||||||||
---|---|---|---|---|---|---|---|---|---|---|
No. | Name | SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
054 | UKMSA01S | 75.78 | 15.19 | 1.39 | 0.05 | 0.04 | 0.06 | 3.11 | 2.22 | 1.93 |
055 | UKMH_02A | 73.19 | 14.44 | 0.80 | 0.02 | 1.63 | 0.13 | 1.93 | 4.24 | 3.47 |
056 | UKMS_03A | 75.89 | 15.25 | 0.97 | 0.05 | 0.38 | 0.15 | 2.48 | 2.47 | 2.17 |
074 | USKS401A | 77.40 | 15.12 | 0.77 | 0.01 | 0.09 | 0.11 | 0.09 | 3.36 | 2.57 |
075 | USK3_02A | 77.27 | 15.51 | 0.66 | 0.01 | 0.09 | 0.13 | 0.07 | 3.05 | 2.77 |
076 | USKH403A | 76.90 | 15.35 | 0.78 | 0.01 | 0.08 | 0.16 | 0.07 | 3.80 | 2.36 |
084 | UKHT201A | 75.59 | 15.20 | 0.45 | 0.02 | 0.04 | 0.12 | 1.42 | 4.67 | 2.19 |
085 | UKHT202A | 78.46 | 14.83 | 0.37 | 0.02 | 0.05 | 0.13 | 0.06 | 2.93 | 2.55 |
086 | UKH_P03A | 74.12 | 14.20 | 0.85 | 0.02 | 1.29 | 0.11 | 2.56 | 4.33 | 2.36 |
087 | UKHXP05A | 79.08 | 14.28 | 0.60 | 0.02 | 0.03 | 0.08 | 0.06 | 2.77 | 2.78 |
088 | UKH3P06A | 78.39 | 14.86 | 0.63 | 0.03 | 0.06 | 0.10 | 0.06 | 2.20 | 3.36 |
091 | KKS__01A | 78.63 | 14.86 | 0.55 | 0.02 | 0.03 | 0.11 | 0.06 | 2.86 | 2.68 |
092 | KKSHP03A | 79.73 | 14.11 | 0.51 | 0.02 | 0.05 | 0.09 | 0.13 | 3.42 | 1.84 |
093 | KKSHP04S | 80.35 | 13.03 | 0.79 | 0.02 | 0.05 | 0.13 | 0.09 | 3.48 | 1.95 |
094 | KKSHP05A | 75.72 | 14.69 | 0.86 | 0.02 | 0.88 | 0.21 | 0.76 | 3.13 | 3.56 |
095 | KKSHA06A | 77.74 | 14.47 | 0.87 | 0.02 | 0.30 | 0.29 | 0.08 | 3.07 | 3.01 |
096 | KKS__07A | 77.11 | 14.87 | 0.34 | 0.02 | 0.04 | 0.05 | 2.48 | 3.41 | 1.58 |
097 | KKS__08A | 76.34 | 14.69 | 0.68 | 0.02 | 1.13 | 0.12 | 0.31 | 2.65 | 3.82 |
098 | KKS__11A | 79.67 | 14.24 | 0.39 | 0.02 | 0.05 | 0.10 | 0.07 | 2.98 | 2.34 |
099 | KKS__12A | 78.35 | 14.91 | 0.71 | 0.02 | 0.06 | 0.10 | 0.06 | 2.39 | 3.19 |
100 | KKS__13A | 75.03 | 14.75 | 0.90 | 0.02 | 1.75 | 0.14 | 0.04 | 2.19 | 5.00 |
101 | KKS1_14A | 76.85 | 15.31 | 0.81 | 0.00 | 0.91 | 0.12 | 0.12 | 3.44 | 2.13 |
102 | KKS0_15A | 78.38 | 13.88 | 0.80 | 0.02 | 0.14 | 0.20 | 0.07 | 2.97 | 3.41 |
103 | KKS1_16A | 78.44 | 14.58 | 0.71 | 0.02 | 0.10 | 0.14 | 0.07 | 2.88 | 2.76 |
104 | KKSTH17A | 74.98 | 14.97 | 0.78 | 0.02 | 1.21 | 0.14 | 0.20 | 3.33 | 4.18 |
129 | KKNT_02A | 73.88 | 14.19 | 0.85 | 0.02 | 1.51 | 0.14 | 2.21 | 3.93 | 3.15 |
130 | KKNS_03A | 75.05 | 14.83 | 0.87 | 0.02 | 1.79 | 0.14 | 0.05 | 2.28 | 4.74 |
131 | KKN3_04A | 78.87 | 14.83 | 0.60 | 0.02 | 0.03 | 0.11 | 0.03 | 2.12 | 3.19 |
132 | KKH__01A | 76.68 | 15.30 | 0.36 | 0.02 | 0.05 | 0.09 | 2.42 | 3.02 | 1.80 |
133 | KKH__02A | 75.83 | 14.72 | 0.85 | 0.02 | 0.04 | 0.05 | 3.45 | 3.50 | 1.36 |
134 | KHDHP01A | 76.76 | 15.78 | 0.59 | 0.02 | 0.02 | 0.10 | 0.11 | 4.32 | 2.15 |
184 | MKK2_01S | 80.35 | 13.36 | 0.41 | 0.02 | 0.09 | 0.06 | 0.12 | 3.38 | 2.06 |
185 | MKK3_02A | 78.00 | 14.89 | 0.85 | 0.02 | 0.13 | 0.09 | 0.06 | 2.97 | 2.77 |
186 | MKKH_03A | 77.82 | 14.41 | 0.89 | 0.02 | 0.31 | 0.33 | 0.07 | 3.27 | 2.64 |
200 | HTO__01S | 76.03 | 14.86 | 1.26 | 0.05 | 0.13 | 0.03 | 3.86 | 2.32 | 1.30 |
201 | HTO4_02A | 75.83 | 14.59 | 1.40 | 0.05 | 0.06 | 0.11 | 4.19 | 2.27 | 1.31 |
202 | HTOTA03A | 75.53 | 14.95 | 1.16 | 0.05 | 0.04 | 0.12 | 4.02 | 2.34 | 1.53 |
203 | HTOSA04A | 75.85 | 14.53 | 1.46 | 0.05 | 0.06 | 0.10 | 4.07 | 2.30 | 1.32 |
Mineral compositions (wt%) | |||||||
---|---|---|---|---|---|---|---|
No. | Name | Quartz | Sericite | Kaolin mineral | Feldspar | Calcite | Siderite |
054 | UKMSA01S | 45.74 | 9.47 | 7.14 | 37.65 | 0.00 | 0.00 |
055 | UKMH_02A | 35.88 | 42.54 | 8.17 | 9.78 | 2.91 | 0.72 |
056 | UKMS_03A | 46.02 | 23.02 | 8.97 | 21.98 | 0.00 | 0.01 |
074 | USKS401A | 60.79 | 24.59 | 13.30 | 1.03 | 0.25 | 0.04 |
075 | USK3_02A | 54.10 | 31.62 | 12.96 | 1.18 | 0.00 | 0.14 |
076 | USKH403A | 58.83 | 34.07 | 5.09 | 1.20 | 0.41 | 0.40 |
084 | UKHT201A | 46.44 | 24.26 | 11.13 | 18.17 | 0.00 | 0.00 |
085 | UKHT202A | 60.68 | 33.99 | 4.63 | 0.63 | 0.00 | 0.07 |
086 | UKH_P03A | 36.76 | 29.64 | 3.72 | 28.83 | 0.00 | 1.05 |
087 | UKHXP05A | 60.86 | 26.27 | 11.36 | 1.39 | 0.00 | 0.12 |
088 | UKH3P06A | 59.05 | 19.95 | 20.25 | 0.70 | 0.00 | 0.05 |
091 | KKS__01A | 62.01 | 23.85 | 13.07 | 1.07 | 0.00 | 0.00 |
092 | KKSHP03A | 56.89 | 33.34 | 8.51 | 1.11 | 0.00 | 0.15 |
093 | KKSHP04S | 62.06 | 34.32 | 0.87 | 1.95 | 0.00 | 0.80 |
094 | KKSHP05A | 45.79 | 32.97 | 14.44 | 4.71 | 1.60 | 0.49 |
095 | KKSHA06A | 53.11 | 35.62 | 9.19 | 1.43 | 0.00 | 0.65 |
096 | KKS__07A | 47.23 | 25.82 | 6.12 | 20.81 | 0.00 | 0.02 |
097 | KKS__08A | 51.71 | 27.61 | 16.38 | 2.13 | 2.00 | 0.17 |
098 | KKS__11A | 65.40 | 26.88 | 5.89 | 1.19 | 0.49 | 0.15 |
099 | KKS__12A | 60.63 | 19.79 | 18.31 | 0.96 | 0.00 | 0.31 |
100 | KKS__13A | 54.49 | 18.48 | 22.30 | 1.00 | 3.11 | 0.62 |
101 | KKS1_14A | 55.01 | 34.17 | 8.28 | 0.50 | 1.59 | 0.45 |
102 | KKS0_15A | 61.19 | 28.94 | 8.05 | 0.91 | 0.00 | 0.91 |
103 | KKS1_16A | 53.01 | 33.88 | 12.50 | 0.51 | 0.00 | 0.10 |
104 | KKSTH17A | 49.62 | 33.58 | 13.75 | 0.50 | 2.14 | 0.41 |
129 | KKNT_02A | 39.08 | 31.79 | 4.29 | 21.86 | 2.68 | 0.30 |
130 | KKNS_03A | 52.93 | 22.51 | 20.25 | 1.14 | 3.16 | 0.01 |
131 | KKN3_04A | 61.60 | 15.95 | 21.16 | 1.09 | 0.08 | 0.12 |
132 | KKH__01A | 54.20 | 25.10 | 2.47 | 18.20 | 0.00 | 0.03 |
133 | KKH__02A | 43.21 | 14.77 | 2.35 | 39.67 | 0.00 | 0.00 |
134 | KHDHP01A | 58.30 | 37.31 | 0.87 | 3.16 | 0.00 | 0.36 |
184 | MKK2_01S | 63.64 | 28.63 | 6.34 | 1.38 | 0.00 | 0.01 |
185 | MKK3_02A | 60.13 | 27.10 | 11.70 | 1.00 | 0.00 | 0.07 |
186 | MKKH_03A | 48.18 | 45.18 | 5.20 | 0.78 | 0.32 | 0.34 |
200 | HTO__01S | 41.64 | 18.89 | 0.30 | 39.17 | 0.00 | 0.00 |
201 | HTO4_02A | 47.41 | 8.32 | 1.56 | 42.36 | 0.35 | 0.00 |
202 | HTOTA03A | 47.93 | 10.25 | 1.67 | 39.86 | 0.29 | 0.00 |
203 | HTOSA04A | 40.23 | 18.85 | 0.87 | 39.76 | 0.29 | 0.00 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. No. | Name | LT | (wt%) L400 | (wt%) X | Y | Z | Whiteness | (Hunter) L | a | b | Whiteness | (Lab) 054 | UKMSA01S | 2.28 | 1.65 | 51.41 | 46.07 | 29.38 | 24.90 | 67.87 | 16.42 | 21.85 | 57.82
| 055 | UKMH_02A | 3.75 | 3.35 | 61.36 | 61.37 | 64.74 | 54.86 | 78.34 | 2.72 | 5.84 | 77.40
| 056 | UKMS_03A | 2.56 | 1.99 | 61.93 | 57.05 | 38.64 | 32.75 | 75.53 | 14.18 | 22.54 | 63.84
| 074 | USKS401A | 3.26 | 2.33 | 61.85 | 57.14 | 40.23 | 34.09 | 75.59 | 13.77 | 21.36 | 64.76
| 075 | USK3_02A | 3.56 | 2.54 | 62.88 | 58.86 | 47.05 | 39.87 | 76.72 | 12.04 | 17.34 | 68.57
| 076 | USKH403A | 3.31 | 2.16 | 62.80 | 62.10 | 64.55 | 54.70 | 78.80 | 4.34 | 6.60 | 77.38
| 084 | UKHT201A | 2.69 | 2.07 | 74.30 | 71.69 | 68.99 | 58.47 | 84.67 | 8.47 | 10.96 | 79.34
| 085 | UKHT202A | 3.46 | 2.38 | 81.19 | 80.27 | 85.18 | 72.19 | 89.59 | 4.97 | 6.35 | 86.84
| 086 | UKH_P03A | 2.70 | 2.25 | 60.60 | 59.68 | 61.96 | 52.51 | 77.25 | 4.83 | 6.52 | 75.85
| 087 | UKHXP05A | 3.26 | 2.62 | 75.90 | 75.35 | 79.18 | 67.10 | 86.80 | 4.17 | 6.68 | 84.63
| 088 | UKH3P06A | 3.91 | 3.17 | 70.24 | 67.86 | 63.68 | 53.97 | 82.38 | 8.04 | 11.83 | 77.30
| 091 | KKS__01A | 3.05 | 2.54 | 70.22 | 67.65 | 63.60 | 53.90 | 82.25 | 8.46 | 11.73 | 77.11
| 092 | KKSHP03A | 2.09 | 1.72 | 67.48 | 64.77 | 61.36 | 52.00 | 80.48 | 8.83 | 11.13 | 75.86
| 093 | KKSHP04S | 2.19 | 1.86 | 64.63 | 64.27 | 69.16 | 58.61 | 80.17 | 3.61 | 4.97 | 79.24
| 094 | KKSHP05A | 3.91 | 3.41 | 62.13 | 61.22 | 62.57 | 53.03 | 78.24 | 4.81 | 7.36 | 76.53
| 095 | KKSHA06A | 3.33 | 2.85 | 62.56 | 62.00 | 65.22 | 55.27 | 78.74 | 4.03 | 6.01 | 77.54
| 096 | KKS__07A | 1.85 | 1.50 | 83.10 | 83.47 | 88.80 | 75.25 | 91.36 | 2.47 | 6.33 | 89.01
| 097 | KKS__08A | 4.26 | 3.61 | 65.40 | 62.25 | 52.81 | 44.75 | 78.90 | 9.89 | 15.54 | 71.99
| 098 | KKS__11A | 2.64 | 2.23 | 79.45 | 79.67 | 87.45 | 74.11 | 89.26 | 2.68 | 4.39 | 88.09
| 099 | KKS__12A | 3.56 | 3.01 | 64.98 | 63.72 | 65.60 | 55.59 | 79.82 | 5.61 | 7.15 | 77.87
| 100 | KKS__13A | 5.33 | 4.86 | 59.77 | 59.35 | 64.04 | 54.27 | 77.04 | 3.67 | 4.64 | 76.29
| 101 | KKS1_14A | 2.68 | 1.98 | 82.57 | 82.61 | 85.80 | 72.71 | 90.89 | 3.10 | 7.65 | 87.70
| 102 | KKS0_15A | 3.68 | 3.30 | 83.44 | 83.44 | 91.12 | 77.22 | 91.35 | 3.20 | 4.80 | 89.60
| 103 | KKS1_16A | 3.32 | 2.59 | 65.97 | 65.47 | 71.35 | 60.47 | 80.91 | 3.94 | 4.36 | 80.03
| 104 | KKSTH17A | 4.54 | 4.00 | 63.30 | 61.44 | 57.71 | 48.91 | 78.38 | 6.98 | 11.22 | 74.67
| 129 | KKNT_02A | 3.40 | 3.04 | 61.94 | 61.26 | 63.96 | 54.20 | 78.27 | 4.29 | 6.34 | 76.96
| 130 | KKNS_03A | 5.14 | 4.50 | 55.26 | 50.62 | 38.77 | 32.86 | 71.15 | 14.13 | 17.49 | 63.42
| 131 | KKN3_04A | 3.57 | 3.03 | 71.88 | 69.40 | 65.55 | 55.55 | 83.31 | 8.23 | 11.66 | 78.04
| 132 | KKH__01A | 2.26 | 1.65 | 83.00 | 82.81 | 82.89 | 70.25 | 91.00 | 3.56 | 9.69 | 86.30
| 133 | KKH__02A | 1.75 | 1.15 | 61.49 | 56.34 | 38.72 | 32.81 | 75.06 | 14.87 | 21.96 | 63.59
| 134 | KHDHP01A | 2.44 | 2.05 | 74.93 | 73.66 | 71.60 | 60.68 | 85.83 | 5.65 | 10.61 | 81.41
| 184 | MKK2_01S | 2.40 | 1.96 | 76.95 | 76.27 | 76.78 | 65.07 | 87.33 | 4.45 | 9.01 | 83.83
| 185 | MKK3_02A | 3.23 | 2.60 | 58.84 | 54.05 | 41.22 | 34.93 | 73.52 | 14.20 | 18.22 | 64.86
| 186 | MKKH_03A | 3.13 | 2.46 | 58.89 | 56.03 | 48.61 | 41.19 | 74.85 | 9.44 | 13.89 | 69.76
| 200 | HTO__01S | 1.63 | 1.11 | 51.91 | 46.50 | 30.17 | 25.57 | 68.19 | 16.55 | 21.50 | 58.19
| 201 | HTO4_02A | 1.77 | 1.08 | 48.84 | 44.06 | 30.05 | 25.47 | 66.38 | 15.18 | 19.62 | 58.22
| 202 | HTOTA03A | 2.11 | 1.32 | 53.15 | 48.14 | 32.19 | 27.28 | 69.38 | 15.32 | 21.06 | 59.81
| 203 | HTOSA04A | 1.83 | 1.14 | 47.87 | 42.26 | 25.71 | 21.79 | 65.01 | 17.68 | 22.06 | 55.02
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Results of TMA and Colors of the Sintered Samples after Measuring | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SM : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. No. | Name | W10 | (wt%) SM | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 054 | UKMSA01S | 47.0 | 9.91 | 1263 | 1275 | 1270 | 1407 | 14 | 40.97 | 40.96 | 36.44 | 30.88 | 64.00 | 2.27 | 11.04 | 62.28
| 055 | UKMH_02A | 50.4 | 8.20 | 1258 | 1266 | 1258 | 1391 | 13+ | 45.95 | 46.44 | 49.38 | 41.85 | 68.15 | 1.10 | 4.74 | 67.78
| 056 | UKMS_03A | 43.3 | 8.91 | 1302 | 1315 | 1313 | 1463 | 16 | 51.63 | 52.95 | 51.16 | 43.36 | 72.77 | -0.69 | 9.25 | 71.23
| 074 | USKS401A | 50.5 | 6.93 | 1419 | 1429 | 1421 | 1572 | 26 | 58.87 | 60.30 | 64.04 | 54.27 | 77.65 | -0.57 | 5.46 | 76.99
| 075 | USK3_02A | 48.6 | 6.80 | 1407 | 1418 | 1412 | 1565 | 26- | 57.02 | 58.45 | 62.37 | 52.86 | 76.45 | -0.66 | 5.15 | 75.89
| 076 | USKH403A | 52.8 | 8.02 | 1391 | 1399 | 1390 | 1545 | 20+ | 55.82 | 57.12 | 60.82 | 51.54 | 75.58 | -0.43 | 5.19 | 75.03
| 084 | UKHT201A | 44.8 | 6.73 | 1312 | 1331 | 1328 | 1480 | 17 | 65.68 | 66.49 | 73.09 | 61.94 | 81.54 | 1.08 | 3.93 | 81.10
| 085 | UKHT202A | 53.0 | 6.76 | 1434 | 1447 | 1438 | 1585 | 26 | 72.54 | 73.58 | 82.41 | 69.84 | 85.78 | 0.84 | 3.08 | 85.42
| 086 | UKH_P03A | 47.6 | 9.43 | 1236 | 1247 | 1241 | 1366 | 13- | 35.88 | 35.44 | 38.15 | 32.33 | 59.53 | 3.40 | 3.68 | 59.22
| 087 | UKHXP05A | 43.6 | 6.15 | 1440 | 1446 | 1443 | 1589 | 26+ | 56.78 | 57.58 | 64.37 | 54.55 | 75.88 | 0.77 | 2.82 | 75.70
| 088 | UKH3P06A | 42.8 | 6.82 | 1450 | 1460 | 1458 | 1599 | 27- | 62.05 | 62.83 | 69.15 | 58.60 | 79.27 | 1.02 | 3.76 | 78.90
| 091 | KKS__01A | 46.8 | 6.85 | 1446 | 1458 | 1453 | 1596 | 27- | 75.40 | 76.34 | 85.91 | 72.81 | 87.37 | 1.14 | 2.86 | 87.00
| 092 | KKSHP03A | 54.9 | 9.67 | 1428 | 1436 | 1425 | 1575 | 26 | 61.43 | 62.17 | 67.01 | 56.79 | 78.85 | 1.08 | 4.81 | 78.28
| 093 | KKSHP04S | 53.8 | 9.25 | 1409 | 1413 | 1403 | 1557 | 26- | 51.17 | 51.90 | 55.88 | 47.36 | 72.04 | 0.71 | 4.44 | 71.68
| 094 | KKSHP05A | 45.9 | 6.85 | 1312 | 1318 | 1314 | 1464 | 16+ | 47.35 | 47.58 | 49.93 | 42.31 | 68.98 | 1.82 | 5.37 | 68.46
| 095 | KKSHA06A | 49.4 | 7.08 | 1383 | 1390 | 1383 | 1539 | 20+ | 50.22 | 50.88 | 54.62 | 46.29 | 71.33 | 0.84 | 4.53 | 70.96
| 096 | KKS__07A | 52.8 | 7.80 | 1317 | 1334 | 1325 | 1477 | 17 | 68.68 | 69.67 | 76.00 | 64.41 | 83.47 | 0.80 | 4.44 | 82.86
| 097 | KKS__08A | 47.5 | 6.69 | 1349 | 1358 | 1353 | 1508 | 18+ | 60.39 | 61.18 | 67.51 | 57.21 | 78.22 | 0.93 | 3.58 | 77.91
| 098 | KKS__11A | 49.9 | 8.01 | 1444 | 1456 | 1449 | 1593 | 26+ | 70.62 | 71.47 | 79.90 | 67.71 | 84.54 | 1.16 | 3.14 | 84.18
| 099 | KKS__12A | 50.2 | 6.35 | 1456 | 1460 | 1453 | 1595 | 27- | 54.88 | 55.58 | 60.89 | 51.60 | 74.55 | 0.93 | 3.76 | 74.26
| 100 | KKS__13A | 47.8 | 5.50 | 1356 | 1359 | 1353 | 1509 | 18+ | 49.65 | 50.27 | 52.95 | 44.87 | 70.90 | 0.92 | 5.35 | 70.40
| 101 | KKS1_14A | 51.5 | 6.54 | 1429 | 1438 | 1430 | 1579 | 26 | 73.46 | 74.22 | 83.01 | 70.35 | 86.15 | 1.44 | 3.18 | 85.72
| 102 | KKS0_15A | 47.1 | 6.56 | 1510 | 1517 | 1512 | 1629 | 28 | 70.12 | 70.75 | 81.31 | 68.91 | 84.11 | 1.61 | 1.56 | 83.96
| 103 | KKS1_16A | 50.0 | 6.31 | 1435 | 1442 | 1435 | 1583 | 26 | 57.82 | 58.62 | 63.46 | 53.78 | 76.56 | 0.81 | 4.45 | 76.13
| 104 | KKSTH17A | 45.9 | 6.47 | 1331 | 1336 | 1332 | 1485 | 17+ | 52.31 | 52.92 | 55.33 | 46.89 | 72.75 | 1.05 | 5.83 | 72.11
| 129 | KKNT_02A | 46.2 | 9.51 | 1253 | 1264 | 1259 | 1392 | 13+ | 39.44 | 39.47 | 40.98 | 34.73 | 62.83 | 2.11 | 5.30 | 62.39
| 130 | KKNS_03A | 43.9 | 6.23 | 1341 | 1347 | 1344 | 1499 | 18 | 53.73 | 54.97 | 55.54 | 47.07 | 74.14 | -0.39 | 7.48 | 73.08
| 131 | KKN3_04A | 45.5 | 7.30 | 1460 | 1467 | 1463 | 1602 | 27- | 64.37 | 65.82 | 73.70 | 62.46 | 81.13 | -0.35 | 2.93 | 80.90
| 132 | KKH__01A | 45.5 | 8.50 | 1334 | 1350 | 1346 | 1501 | 18 | 67.19 | 68.83 | 74.80 | 63.39 | 82.96 | -0.62 | 4.62 | 82.34
| 133 | KKH__02A | 48.0 | 9.39 | 1259 | 1279 | 1273 | 1412 | 14 | 48.33 | 48.69 | 43.84 | 37.15 | 69.78 | 1.52 | 11.59 | 67.59
| 134 | KHDHP01A | 47.3 | 9.54 | 1392 | 1405 | 1400 | 1554 | 20+ | 63.10 | 64.49 | 69.54 | 58.93 | 80.31 | -0.28 | 4.87 | 79.71
| 184 | MKK2_01S | 54.6 | 8.69 | 1429 | 1437 | 1426 | 1576 | 26 | 65.58 | 67.14 | 74.26 | 62.93 | 81.94 | -0.53 | 3.62 | 81.57
| 185 | MKK3_02A | 50.4 | 7.45 | 1427 | 1435 | 1427 | 1577 | 26 | 68.87 | 70.54 | 79.24 | 67.15 | 83.99 | -0.61 | 2.85 | 83.72
| 186 | MKKH_03A | 52.3 | 6.68 | 1391 | 1398 | 1389 | 1545 | 20+ | 50.57 | 51.91 | 54.91 | 46.53 | 72.05 | -0.80 | 5.25 | 71.55
| 200 | HTO__01S | 53.3 | 10.2 | 1257 | 1267 | 1257 | 1389 | 13+ | 37.77 | 36.40 | 28.52 | 24.17 | 60.33 | 6.16 | 14.21 | 57.42
| 201 | HTO4_02A | 50.4 | 9.27 | 1252 | 1263 | 1255 | 1387 | 13+ | 40.77 | 40.31 | 34.60 | 29.32 | 63.49 | 3.52 | 12.13 | 61.37
| 202 | HTOTA03A | 51.8 | 8.04 | 1264 | 1272 | 1263 | 1398 | 14- | 43.05 | 42.81 | 37.73 | 31.97 | 65.43 | 2.94 | 11.61 | 63.41
| 203 | HTOSA04A | 53.0 | 8.83 | 1249 | 1259 | 1250 | 1378 | 13 | 33.36 | 30.79 | 21.21 | 17.97 | 55.49 | 10.21 | 16.18 | 51.55
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