XRD, TGA and TMA Charts (No.201)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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201 | HTO4_02A | June 11,1981 | Kaigan V. | Ohsako | Harada Tohseki | Right wall | Good rock, Fourth grade ? |
Colors of the milled samples | |||||||
---|---|---|---|---|---|---|---|
X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
62.07 | 60.59 | 43.97 | 37.26 | 77.84 | 6.12 | 21.00 | 68.87 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
75.83 | 14.59 | 1.40 | 0.05 | 0.06 | 0.11 | 4.19 | 2.27 | 1.31 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
47.41 | 8.32 | 1.56 | 42.36 | 0.35 | 0.00 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 1.77 | 1.08 | 48.84 | 44.06 | 30.05 | 25.47 | 66.38 | 15.18 | 19.62 | 58.22
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 50.4 | 9.27 | 1252 | 1263 | 1255 | 1387 | 13+ | 40.77 | 40.31 | 34.60 | 29.32 | 63.49 | 3.52 | 12.13 | 61.37
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