XRD, TGA and TMA Charts (No.104)
| No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
|---|---|---|---|---|---|---|---|
| 104 | KKSTH17A | November 13,1982 | Kaigan V. | Iwaotoshi | Kiyama Tohseki | Inside drift | Low SK, Henshoku (discoloration), SK17 |
| Colors of the milled samples | |||||||
|---|---|---|---|---|---|---|---|
| X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
| 77.63 | 78.17 | 73.32 | 62.14 | 88.41 | 2.00 | 12.72 | 82.68 |
| Chemical compositions (wt%) | ||||||||
|---|---|---|---|---|---|---|---|---|
| SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
| 74.98 | 14.97 | 0.78 | 0.02 | 1.21 | 0.14 | 0.20 | 3.33 | 4.18 |
| Mineral compositions (wt%) | |||||
|---|---|---|---|---|---|
| Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
| 49.62 | 33.58 | 13.75 | 0.50 | 2.14 | 0.41 |
| Results of TGA and Colors of the Powder Samples after Measuring | |||||||||
|---|---|---|---|---|---|---|---|---|---|
The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. | |||||||||
| LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
| 4.54 | 4.00 | 63.30 | 61.44 | 57.71 | 48.91 | 78.38 | 6.98 | 11.22 | 74.67 |
| Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. | ||||||||||||||
| W10 (wt%) | SMax (%) | T0 (°C) | T5 (°C) | TS5 (°C) | TSK (°C) | SK | X | Y | Z | W (Hunter) | L | a | b | W (Lab) |
| 45.9 | 6.47 | 1331 | 1336 | 1332 | 1485 | 17+ | 52.31 | 52.92 | 55.33 | 46.89 | 72.75 | 1.05 | 5.83 | 72.11 |
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