XRD, TGA and TMA Charts (No.096)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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096 | KKS__07A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | In the factory of acid treatment | Product, SK18 |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
85.11 | 85.50 | 92.03 | 77.99 | 92.47 | 2.48 | 5.72 | 90.22 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
77.11 | 14.87 | 0.34 | 0.02 | 0.04 | 0.05 | 2.48 | 3.41 | 1.58 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
47.23 | 25.82 | 6.12 | 20.81 | 0.00 | 0.02 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 1.85 | 1.50 | 83.10 | 83.47 | 88.80 | 75.25 | 91.36 | 2.47 | 6.33 | 89.01
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 52.8 | 7.80 | 1317 | 1334 | 1325 | 1477 | 17 | 68.68 | 69.67 | 76.00 | 64.41 | 83.47 | 0.80 | 4.44 | 82.86
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