Henshoku (Discoloration) pottery stone, 35 samples
Colors of the milled samples |
Chemical compositions |
Mineral compositions |
Results of TGA & Colors of the powder samples after measuring |
Results of TMA & Colors of the sintered samples after measuring |
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
---|---|---|---|---|---|---|---|
005 | USGH_05A | March 29, 1980 | Sarayama V. | Gohtsu | Ueda Tohseki | North | Hensyoku/ Tamamono (discoloration), Siderite(+) |
009 | USGH_09A | July 16, 1980 | Sarayama V. | Gohtsu | Ueda Tohseki | Lower level | Hensyoku/ Tamamono (discoloration) ? |
013 | USGH_14A | November 13, 1982 | Sarayama V. | Gohtsu | Ueda Tohseki | Lower level/right | Tamamono/ Henshoku (discoloration), hard |
014 | USGH_15A | November 13, 1982 | Sarayama V. | Gohtsu | Ueda Tohseki | Lower level/right | Tamamono/ Henshoku (discoloration), soft |
023 | USDH_04S | March 29, 1980 | Sarayama V. | Denbeekoba | Ueda Tohseki | ? | Henshoku (discoloration) |
034 | USDH_15A | June 11, 1981 | Sarayama V. | Denbeekoba | Ueda Tohseki | Second level/left-upper | High SK, Henshoku (discoloration) |
037 | USDH_18A | June 11, 1981 | Sarayama V. | Denbeekoba | Ueda Tohseki | Middle level/upper-left | Henshoku (discoloration), SK26 |
038 | USDH_19A | November 13, 1982 | Sarayama V. | Denbeekoba | Ueda Tohseki | Upper level/center | Henshoku (discoloration), deep color sppoted |
039 | USDH_20A | November 13, 1982 | Sarayama V. | Denbeekoba | Ueda Tohseki | Upper level/right | Henshoku (discoloration), boundary of Shima (stripes) |
048 | USIH_09A | March 30, 1982 | Sarayama V. | Iguchiyama | Ueda Tohseki | Cliff/right, lower of upper level | Look like Henshoku (discoloration) |
049 | USIH_10A | March 30, 1982 | Sarayama V. | Iguchiyama | Ueda Tohseki | Cliff/right, lower of upper level | Henshoku (discoloration) |
051 | USIH_12A | November 15, 1983 | Sarayama V. | Iguchiyama | Ueda Tohseki | Second level | Raw material of Amakusa clay ?, Henshoku (discoloration) |
052 | USIH_13A | November 15, 1983 | Sarayama V. | Iguchiyama | Ueda Tohseki | Second level | Raw material of Amakusa clay ?, Henshoku (discoloration) |
067 | USTH_01A | March 30, 1982 | Sarayama V. | Toboshi | Ueda Tohseki | Center/left | Henshoku (discoloration) |
068 | UST__02A | March 30, 1982 | Sarayama V. | Toboshi | Ueda Tohseki | Right of USTH_01A | Look like Henshoku (discoloration) |
077 | USSH_01A | March 30, 1982 | Sarayama V. | Tsurugigasako | Ueda Tohseki | Inside drift | High SK Henshoku (discoloration) with white color |
078 | USSH_02A | March 30, 1982 | Sarayama V. | Tsurugigasako | Ueda Tohseki | Inside drift | High SK Henshoku (discoloration) with white color |
079 | USSH_03A | March 30, 1982 | Sarayama V. | Tsurugigasako | Ueda Tohseki | Outside drift | =USSH_01A (SK26) |
055 | UKMH_02A | July 16, 1980 | Kaigan V. | Michitanosako | Ueda Tohseki | Stack | Henshoku (discoloration) |
092 | KKSHP03A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Center | Henshoku (discoloration), FeS(+), Fe2O3=1wt% |
093 | KKSHP04S | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Inside drift/right | Henshoku (discoloration), FeS(+) |
094 | KKSHP05A | July 16, 1980 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Outside stock | Henshoku (discoloration), FeS(+) |
095 | KKSHA06A | March 26, 1981 | Kaigan V. | Shimizuotoshi | Kiyama Tohseki | Shinyama fifth drift | Henshoku (discoloration) A, SK20-25 |
104 | KKSTH17A | November 13, 1982 | Kaigan V. | Iwaotoshi | Kiyama Tohseki | Inside drift | Low SK, Henshoku (discoloration), SK17 |
134 | KHDHP01A | November 15, 1983 | Kaigan V. | Tanohira | Kiyama Tohseki | Open cut | FeS(+), Henshoku (discoloration), SK26-27 |
186 | MKKH_03A | December 1, 1980 | Kaigan V. | Kawanohata | Matsuzaki Tohseki | Stock yard | Henshoku(discoloration) |
057 | UMOH_01A | June 11, 1981 | Murayama V. | Odatoko Furuyashiki | Ueda Tohseki | Lower drift, upper working face/center | Good rock, Henshoku (discoloration) |
157 | NMSH_03A | November 15, 1983 | Murayama V. | Shinden | Nishizima Tohseki | Shinden drift, under 30m from Yamanokohira incline shaft | Henshoku (discoloration) |
159 | NMNH_01A | March 26, 1981 | Murayama V. | Nihonmatsu | Nishizima Tohseki | Nihonmatsu drift | Group of Henshoku (discoloration) |
161 | NMYH_03S | March 26, 1981 | Murayama V. | Yamanokohira | Nishizima Tohseki | Stock yard, from Hashiriochi ? | Henshoku (discoloration), SK26 |
164 | NMYTH02A | March 26, 1981 | Murayama V. | Yamanokohira | Nishizima Tohseki | Stock yard | Low SK, Henshoku (discoloration), SK15-16 |
165 | NMYH_04A | March 26, 1981 | Murayama V. | Yamanokohira | Nishizima Tohseki | ? | High SK, discoloration surface |
166 | NMYH_05A | March 26, 1981 | Murayama V. | Yamanokohira | Nishizima Tohseki | ? | High SK, no discoloration surface |
173 | HFIH_01S | March 26, 1981 | Fukami V. | Fukami | Hisatsune Tohseki | Inside drift/right/forth working face | Henshoku (discoloration) |
195 | SFDH_02A | March 26, 1981 | Fukami V. | Fukami | Shin-ei Tohseki | Stock yard | Henshoku (discoloration) |
Colors of the milled samples | |||||||||
---|---|---|---|---|---|---|---|---|---|
No. | Name | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
005 | USGH_05A | 69.32 | 67.84 | 63.51 | 53.82 | 82.37 | 6.09 | 11.94 | 77.85 |
009 | USGH_09A | 78.48 | 79.12 | 80.05 | 67.84 | 88.95 | 1.83 | 8.91 | 85.69 |
013 | USGH_14A | 81.52 | 82.95 | 87.60 | 74.24 | 91.08 | 0.39 | 6.73 | 88.82 |
014 | USGH_15A | 80.37 | 81.74 | 86.31 | 73.14 | 90.41 | 0.46 | 6.69 | 88.30 |
023 | USDH_04S | 56.07 | 55.74 | 53.68 | 45.49 | 74.66 | 3.40 | 9.63 | 72.68 |
034 | USDH_15A | 67.68 | 67.77 | 66.09 | 56.01 | 82.32 | 2.69 | 10.03 | 79.50 |
037 | USDH_18A | 77.83 | 78.51 | 79.27 | 67.18 | 88.61 | 1.73 | 8.98 | 85.39 |
038 | USDH_19A | 77.93 | 78.81 | 79.68 | 67.53 | 88.77 | 1.34 | 8.93 | 85.60 |
039 | USDH_20A | 71.79 | 72.30 | 67.96 | 57.59 | 85.03 | 1.91 | 12.13 | 80.64 |
048 | USIH_09A | 85.09 | 86.10 | 95.07 | 80.57 | 92.79 | 1.30 | 4.21 | 91.55 |
049 | USIH_10A | 84.75 | 85.57 | 94.97 | 80.48 | 92.50 | 1.66 | 3.88 | 91.40 |
051 | USIH_12A | 53.45 | 52.52 | 47.22 | 40.02 | 72.47 | 4.83 | 12.10 | 69.54 |
052 | USIH_13A | 83.66 | 84.37 | 86.26 | 73.10 | 91.85 | 1.84 | 8.62 | 88.00 |
067 | USTH_01A | 71.76 | 71.08 | 69.70 | 59.07 | 84.31 | 4.39 | 10.00 | 80.88 |
068 | UST__02A | 74.60 | 73.73 | 67.82 | 57.47 | 85.87 | 4.81 | 13.28 | 80.02 |
077 | USSH_01A | 73.33 | 73.81 | 73.21 | 62.04 | 85.91 | 2.01 | 9.62 | 82.83 |
078 | USSH_02A | 76.24 | 76.62 | 80.98 | 68.63 | 87.53 | 2.29 | 6.42 | 85.79 |
079 | USSH_03A | 75.30 | 75.50 | 79.04 | 66.98 | 86.89 | 2.63 | 6.89 | 84.96 |
055 | UKMH_02A | 82.53 | 83.11 | 88.57 | 75.06 | 91.16 | 2.06 | 6.21 | 89.01 |
092 | KKSHP03A | 76.95 | 76.46 | 71.21 | 60.35 | 87.44 | 4.06 | 12.92 | 81.53 |
093 | KKSHP04S | 77.96 | 77.81 | 82.57 | 69.97 | 88.21 | 3.39 | 6.25 | 86.23 |
094 | KKSHP05A | 79.42 | 79.39 | 80.67 | 68.36 | 89.10 | 3.18 | 8.69 | 85.70 |
095 | KKSHA06A | 82.95 | 83.24 | 90.12 | 76.37 | 91.24 | 2.63 | 5.30 | 89.43 |
104 | KKSTH17A | 77.63 | 78.17 | 73.32 | 62.14 | 88.41 | 2.00 | 12.72 | 82.68 |
134 | KHDHP01A | 78.94 | 79.49 | 78.92 | 66.88 | 89.16 | 2.02 | 9.93 | 85.16 |
186 | MKKH_03A | 72.34 | 71.30 | 61.87 | 52.43 | 84.44 | 5.15 | 15.66 | 77.33 |
057 | UMOH_01A | 86.68 | 87.47 | 97.66 | 82.76 | 93.53 | 1.77 | 3.56 | 92.40 |
157 | NMSH_03A | 77.62 | 77.99 | 78.94 | 66.90 | 88.31 | 2.34 | 8.82 | 85.17 |
159 | NMNH_01A | 81.29 | 82.00 | 86.64 | 73.42 | 90.55 | 1.77 | 6.66 | 88.31 |
161 | NMYH_03S | 76.39 | 76.28 | 75.34 | 63.85 | 87.34 | 3.28 | 9.99 | 83.54 |
164 | NMYTH02A | 83.53 | 84.20 | 90.16 | 76.41 | 91.76 | 1.91 | 5.98 | 89.64 |
165 | NMYH_04A | 75.75 | 75.82 | 79.39 | 67.28 | 87.07 | 2.90 | 6.89 | 85.07 |
166 | NMYH_05A | 80.49 | 80.60 | 78.84 | 66.81 | 89.78 | 2.92 | 10.78 | 84.86 |
173 | HFIH_01S | 85.82 | 86.80 | 97.60 | 82.71 | 93.17 | 1.38 | 3.11 | 92.37 |
195 | SFDH_02A | 79.43 | 79.21 | 77.96 | 66.07 | 89.00 | 3.56 | 10.36 | 84.47 |
Chemical compositions (wt%) | ||||||||||
---|---|---|---|---|---|---|---|---|---|---|
No. | Name | SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
005 | USGH_05A | 74.81 | 14.78 | 0.93 | 0.01 | 1.18 | 0.12 | 2.61 | 2.12 | 3.16 |
009 | USGH_09A | 73.65 | 14.75 | 0.70 | 0.01 | 1.43 | 0.06 | 3.53 | 3.13 | 2.57 |
013 | USGH_14A | 76.97 | 15.22 | 0.85 | 0.01 | 0.10 | 0.15 | 1.00 | 2.20 | 3.10 |
014 | USGH_15A | 76.54 | 15.66 | 0.84 | 0.01 | 0.10 | 0.16 | 0.88 | 2.33 | 3.06 |
023 | USDH_04S | 77.63 | 14.51 | 1.19 | 0.01 | 0.14 | 0.10 | 0.09 | 3.80 | 2.13 |
034 | USDH_15A | 78.31 | 14.84 | 0.63 | 0.01 | 0.11 | 0.09 | 0.08 | 3.54 | 2.04 |
037 | USDH_18A | 77.64 | 14.90 | 0.77 | 0.01 | 0.15 | 0.10 | 0.08 | 3.36 | 2.46 |
038 | USDH_19A | 74.03 | 15.04 | 0.78 | 0.01 | 2.04 | 0.12 | 0.06 | 3.68 | 3.77 |
039 | USDH_20A | 77.00 | 15.45 | 0.76 | 0.01 | 0.13 | 0.11 | 0.09 | 3.82 | 2.17 |
048 | USIH_09A | 77.88 | 15.19 | 0.33 | 0.01 | 0.43 | 0.12 | 0.06 | 3.13 | 2.52 |
049 | USIH_10A | 77.94 | 15.41 | 0.34 | 0.01 | 0.06 | 0.15 | 0.09 | 3.09 | 2.58 |
051 | USIH_12A | 75.40 | 15.00 | 2.36 | 0.01 | 0.16 | 0.17 | 0.10 | 3.44 | 2.89 |
052 | USIH_13A | 77.06 | 15.75 | 0.40 | 0.01 | 0.06 | 0.18 | 0.09 | 3.47 | 2.55 |
067 | USTH_01A | 77.09 | 15.49 | 0.85 | 0.01 | 0.08 | 0.11 | 0.09 | 3.17 | 2.86 |
068 | UST__02A | 77.85 | 15.16 | 0.69 | 0.01 | 0.09 | 0.11 | 0.10 | 3.04 | 2.56 |
077 | USSH_01A | 78.23 | 14.69 | 0.78 | 0.01 | 0.08 | 0.15 | 0.09 | 3.09 | 2.52 |
078 | USSH_02A | 79.21 | 14.12 | 0.71 | 0.01 | 0.08 | 0.15 | 0.03 | 2.94 | 2.36 |
079 | USSH_03A | 79.02 | 14.31 | 0.74 | 0.01 | 0.07 | 0.13 | 0.06 | 3.20 | 2.17 |
055 | UKMH_02A | 73.19 | 14.44 | 0.80 | 0.02 | 1.63 | 0.13 | 1.93 | 4.24 | 3.47 |
092 | KKSHP03A | 79.73 | 14.11 | 0.51 | 0.02 | 0.05 | 0.09 | 0.13 | 3.42 | 1.84 |
093 | KKSHP04S | 80.35 | 13.03 | 0.79 | 0.02 | 0.05 | 0.13 | 0.09 | 3.48 | 1.95 |
094 | KKSHP05A | 75.72 | 14.69 | 0.86 | 0.02 | 0.88 | 0.21 | 0.76 | 3.13 | 3.56 |
095 | KKSHA06A | 77.74 | 14.47 | 0.87 | 0.02 | 0.30 | 0.29 | 0.08 | 3.07 | 3.01 |
104 | KKSTH17A | 74.98 | 14.97 | 0.78 | 0.02 | 1.21 | 0.14 | 0.20 | 3.33 | 4.18 |
134 | KHDHP01A | 76.76 | 15.78 | 0.59 | 0.02 | 0.02 | 0.10 | 0.11 | 4.32 | 2.15 |
186 | MKKH_03A | 77.82 | 14.41 | 0.89 | 0.02 | 0.31 | 0.33 | 0.07 | 3.27 | 2.64 |
057 | UMOH_01A | 77.84 | 15.62 | 0.28 | 0.02 | 0.06 | 0.07 | 0.10 | 3.03 | 2.85 |
157 | NMSH_03A | 75.47 | 14.51 | 0.88 | 0.02 | 0.07 | 0.08 | 3.18 | 4.17 | 1.44 |
159 | NMNH_01A | 73.24 | 14.88 | 0.83 | 0.02 | 2.33 | 0.30 | 0.30 | 2.94 | 4.67 |
161 | NMYH_03S | 78.44 | 14.51 | 0.80 | 0.02 | 0.05 | 0.13 | 0.08 | 2.83 | 2.95 |
164 | NMYTH02A | 76.32 | 15.71 | 0.92 | 0.02 | 0.19 | 0.23 | 0.07 | 3.16 | 3.10 |
165 | NMYH_04A | 77.36 | 14.99 | 1.02 | 0.02 | 0.08 | 0.11 | 0.29 | 2.72 | 3.23 |
166 | NMYH_05A | 77.68 | 15.48 | 0.50 | 0.02 | 0.05 | 0.09 | 0.08 | 2.73 | 3.17 |
173 | HFIH_01S | 79.03 | 14.87 | 0.20 | 0.04 | 0.05 | 0.13 | 0.07 | 0.48 | 4.75 |
195 | SFDH_02A | 78.80 | 15.06 | 0.37 | 0.04 | 0.07 | 0.10 | 0.06 | 0.63 | 4.52 |
Mineral compositions (wt%) | |||||||
---|---|---|---|---|---|---|---|
No. | Name | Quartz | Sericite | Kaolin mineral | Feldspar | Calcite | Siderite |
005 | USGH_05A | 40.40 | 25.77 | 11.93 | 19.81 | 2.09 | 0.00 |
009 | USGH_09A | 41.30 | 18.56 | 4.86 | 32.78 | 2.50 | 0.00 |
013 | USGH_14A | 48.40 | 26.74 | 18.54 | 5.93 | 0.00 | 0.39 |
014 | USGH_15A | 49.21 | 27.82 | 17.06 | 5.50 | 0.00 | 0.41 |
023 | USDH_04S | 51.64 | 46.52 | 0.76 | 0.67 | 0.00 | 0.41 |
034 | USDH_15A | 57.94 | 33.86 | 7.03 | 0.77 | 0.30 | 0.10 |
037 | USDH_18A | 52.89 | 37.31 | 8.28 | 1.08 | 0.00 | 0.44 |
038 | USDH_19A | 42.60 | 46.97 | 5.66 | 0.50 | 3.62 | 0.65 |
039 | USDH_20A | 50.99 | 43.84 | 3.72 | 1.00 | 0.37 | 0.08 |
048 | USIH_09A | 55.04 | 32.28 | 12.16 | 0.52 | 0.00 | 0.00 |
049 | USIH_10A | 60.52 | 24.92 | 13.53 | 0.89 | 0.00 | 0.14 |
051 | USIH_12A | 43.29 | 46.02 | 9.54 | 0.86 | 0.00 | 0.29 |
052 | USIH_13A | 56.90 | 30.61 | 11.13 | 1.17 | 0.00 | 0.19 |
067 | USTH_01A | 52.54 | 30.38 | 16.03 | 0.67 | 0.00 | 0.38 |
068 | UST__02A | 56.89 | 33.34 | 8.51 | 1.11 | 0.00 | 0.15 |
077 | USSH_01A | 55.67 | 33.25 | 9.19 | 1.44 | 0.00 | 0.45 |
078 | USSH_02A | 54.73 | 36.68 | 7.14 | 1.01 | 0.00 | 0.44 |
079 | USSH_03A | 55.11 | 36.27 | 7.03 | 1.33 | 0.00 | 0.26 |
055 | UKMH_02A | 35.88 | 42.54 | 8.17 | 9.78 | 2.91 | 0.72 |
092 | KKSHP03A | 56.89 | 33.34 | 8.51 | 1.11 | 0.00 | 0.15 |
093 | KKSHP04S | 62.06 | 34.32 | 0.87 | 1.95 | 0.00 | 0.80 |
094 | KKSHP05A | 45.79 | 32.97 | 14.44 | 4.71 | 1.60 | 0.49 |
095 | KKSHA06A | 53.11 | 35.62 | 9.19 | 1.43 | 0.00 | 0.65 |
104 | KKSTH17A | 49.62 | 33.58 | 13.75 | 0.50 | 2.14 | 0.41 |
134 | KHDHP01A | 58.30 | 37.31 | 0.87 | 3.16 | 0.00 | 0.36 |
186 | MKKH_03A | 48.18 | 45.18 | 5.20 | 0.78 | 0.32 | 0.34 |
057 | UMOH_01A | 54.83 | 28.29 | 16.38 | 0.50 | 0.00 | 0.00 |
157 | NMSH_03A | 32.65 | 43.45 | 1.44 | 22.02 | 0.00 | 0.44 |
159 | NMNH_01A | 44.39 | 34.80 | 15.69 | 0.55 | 4.12 | 0.45 |
161 | NMYH_03S | 56.47 | 27.07 | 14.44 | 1.25 | 0.00 | 0.77 |
164 | NMYTH02A | 57.31 | 28.64 | 11.82 | 0.83 | 0.43 | 0.97 |
165 | NMYH_04A | 53.42 | 31.07 | 10.79 | 4.43 | 0.00 | 0.29 |
166 | NMYH_05A | 58.67 | 22.71 | 17.97 | 0.50 | 0.07 | 0.08 |
173 | HFIH_01S | 61.80 | 0.01 | 37.69 | 0.50 | 0.00 | 0.00 |
195 | SFDH_02A | 56.48 | 11.40 | 31.54 | 0.50 | 0.00 | 0.08 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1,000°C.
LT : Total weight loss, L400 : Weight loss of 400-1,000°C. No. | Name | LT | (wt%) L400 | (wt%) X | Y | Z | Whiteness | (Hunter) L | a | b | Whiteness | (Lab) 005 | USGH_05A | 3.62 | 2.98 | 62.66 | 60.52 | 57.10 | 48.39 | 77.79 | 7.63 | 10.94 | 74.10
| 009 | USGH_09A | 2.91 | 2.44 | 66.04 | 65.11 | 65.81 | 55.77 | 80.69 | 4.88 | 8.13 | 78.49
| 013 | USGH_14A | 3.79 | 2.91 | 67.43 | 66.99 | 72.46 | 61.41 | 81.85 | 3.82 | 4.80 | 80.84
| 014 | USGH_15A | 3.77 | 2.89 | 67.18 | 66.76 | 72.04 | 61.05 | 81.71 | 3.78 | 4.92 | 80.68
| 023 | USDH_04S | 2.79 | 1.91 | 52.77 | 51.92 | 51.30 | 45.49 | 72.06 | 4.63 | 8.23 | 70.50
| 034 | USDH_15A | 2.66 | 1.91 | 64.46 | 63.86 | 64.31 | 54.50 | 79.91 | 4.14 | 8.22 | 77.90
| 037 | USDH_18A | 3.28 | 2.28 | 61.36 | 60.96 | 65.11 | 55.18 | 78.08 | 3.65 | 5.21 | 77.17
| 038 | USDH_19A | 4.48 | 3.59 | 60.14 | 59.81 | 62.37 | 52.86 | 77.34 | 3.47 | 6.32 | 76.22
| 039 | USDH_20A | 2.82 | 1.99 | 64.33 | 63.29 | 61.77 | 52.35 | 79.56 | 5.12 | 9.65 | 76.82
| 048 | USIH_09A | 3.07 | 2.41 | 84.53 | 85.80 | 92.65 | 78.52 | 92.63 | 0.79 | 5.54 | 90.75
| 049 | USIH_10A | 3.12 | 2.48 | 83.97 | 85.04 | 91.51 | 77.55 | 92.22 | 1.16 | 5.72 | 90.27
| 051 | USIH_12A | 3.74 | 2.57 | 43.14 | 41.88 | 38.05 | 32.25 | 64.71 | 5.74 | 10.44 | 62.76
| 052 | USIH_13A | 3.24 | 2.42 | 82.30 | 83.60 | 87.05 | 73.77 | 91.43 | 0.66 | 7.56 | 88.56
| 067 | USTH_01A | 3.34 | 2.70 | 64.62 | 63.83 | 64.91 | 55.01 | 79.89 | 4.56 | 7.76 | 77.97
| 068 | UST__02A | 3.16 | 2.40 | 66.11 | 63.94 | 59.83 | 50.70 | 79.96 | 7.64 | 11.61 | 75.61
| 077 | USSH_01A | 3.09 | 2.35 | 63.89 | 62.84 | 63.61 | 53.91 | 79.27 | 5.14 | 7.91 | 77.22
| 078 | USSH_02A | 2.96 | 2.14 | 67.25 | 66.81 | 71.50 | 60.59 | 81.74 | 3.82 | 5.35 | 80.59
| 079 | USSH_03A | 2.70 | 2.02 | 65.01 | 64.60 | 69.03 | 58.50 | 80.37 | 3.72 | 5.34 | 79.32
| 055 | UKMH_02A | 3.75 | 3.35 | 61.36 | 61.37 | 64.74 | 54.86 | 78.34 | 2.72 | 5.84 | 77.40
| 092 | KKSHP03A | 2.09 | 1.72 | 67.48 | 64.77 | 61.36 | 52.00 | 80.48 | 8.83 | 11.13 | 75.86
| 093 | KKSHP04S | 2.19 | 1.86 | 64.63 | 64.27 | 69.16 | 58.61 | 80.17 | 3.61 | 4.97 | 79.24
| 094 | KKSHP05A | 3.91 | 3.41 | 62.13 | 61.22 | 62.57 | 53.03 | 78.24 | 4.81 | 7.36 | 76.53
| 095 | KKSHA06A | 3.33 | 2.85 | 62.56 | 62.00 | 65.22 | 55.27 | 78.74 | 4.03 | 6.01 | 77.54
| 104 | KKSTH17A | 4.54 | 4.00 | 63.30 | 61.44 | 57.71 | 48.91 | 78.38 | 6.98 | 11.22 | 74.67
| 134 | KHDHP01A | 2.44 | 2.05 | 74.93 | 73.66 | 71.60 | 60.68 | 85.83 | 5.65 | 10.61 | 81.41
| 186 | MKKH_03A | 3.13 | 2.46 | 58.89 | 56.03 | 48.61 | 41.19 | 74.85 | 9.44 | 13.89 | 69.76
| 057 | UMOH_01A | 3.14 | 2.80 | 85.76 | 86.51 | 94.75 | 80.30 | 93.01 | 1.82 | 4.71 | 91.38
| 157 | NMSH_03A | 1.80 | 1.30 | 62.61 | 61.47 | 62.47 | 52.94 | 78.40 | 5.34 | 7.64 | 76.48
| 159 | NMNH_01A | 5.44 | 4.58 | 57.80 | 57.89 | 61.80 | 52.37 | 76.09 | 2.45 | 5.10 | 75.42
| 161 | NMYH_03S | 3.38 | 2.80 | 63.84 | 62.33 | 62.94 | 53.34 | 78.95 | 6.18 | 8.00 | 76.65
| 164 | NMYTH02A | 3.62 | 2.96 | 62.83 | 62.03 | 65.91 | 55.86 | 78.76 | 4.57 | 5.51 | 77.58
| 165 | NMYH_04A | 3.64 | 3.07 | 59.60 | 59.00 | 63.64 | 53.93 | 76.81 | 4.08 | 4.64 | 76.00
| 166 | NMYH_05A | 3.63 | 3.04 | 73.52 | 71.12 | 70.27 | 59.55 | 84.33 | 8.03 | 9.63 | 79.93
| 173 | HFIH_01S | 5.38 | 4.60 | 85.23 | 86.10 | 92.33 | 78.25 | 92.79 | 1.57 | 5.96 | 90.52
| 195 | SFDH_02A | 5.17 | 4.31 | 68.43 | 66.70 | 64.82 | 54.93 | 81.67 | 6.64 | 10.11 | 78.04
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SM : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. No. | Name | W10 | (wt%) SM | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 005 | USGH_05A | 43.3 | 6.88 | 1263 | 1269 | 1267 | 1403 | 14- | 46.03 | 46.33 | 47.98 | 40.66 | 68.07 | 1.60 | 5.85 | 67.50
| 009 | USGH_09A | 49.9 | 9.02 | 1233 | 1245 | 1238 | 1361 | 12+ | 37.75 | 37.52 | 38.96 | 33.02 | 61.25 | 2.81 | 5.17 | 60.81
| 013 | USGH_14A | 43.7 | 6.38 | 1378 | 1385 | 1382 | 1538 | 20+ | 47.91 | 48.79 | 52.82 | 44.76 | 69.85 | 0.20 | 4.06 | 69.58
| 014 | USGH_15A | 40.9 | 10.0 | 1376 | 1382 | 1381 | 1537 | 20 | 50.82 | 51.72 | 54.52 | 46.20 | 71.92 | 0.28 | 5.39 | 71.40
| 023 | USDH_04S | 49.1 | 6.45 | 1374 | 1380 | 1373 | 1530 | 20 | 43.21 | 43.94 | 46.08 | 39.05 | 66.29 | 0.35 | 5.19 | 65.89
| 034 | USDH_15A | 50.7 | 6.55 | 1411 | 1418 | 1410 | 1563 | 26- | 58.68 | 60.07 | 64.91 | 55.01 | 77.50 | -0.49 | 4.60 | 77.03
| 037 | USDH_18A | 48.6 | 5.57 | 1387 | 1397 | 1391 | 1546 | 20+ | 52.13 | 53.38 | 57.53 | 48.75 | 73.06 | -0.50 | 4.46 | 72.69
| 038 | USDH_19A | 53.1 | 6.52 | 1330 | 1333 | 1323 | 1476 | 17- | 51.48 | 52.28 | 54.03 | 45.79 | 72.30 | 0.56 | 6.31 | 71.59
| 039 | USDH_20A | 49.9 | 7.87 | 1382 | 1393 | 1386 | 1542 | 20+ | 53.83 | 55.14 | 59.29 | 50.25 | 74.26 | -0.55 | 4.64 | 73.84
| 048 | USIH_09A | 47.9 | 8.98 | 1448 | 1458 | 1452 | 1595 | 27- | 72.17 | 73.93 | 83.06 | 70.39 | 85.98 | -0.64 | 2.91 | 85.67
| 049 | USIH_10A | 47.4 | 6.55 | 1439 | 1452 | 1447 | 1591 | 26+ | 72.32 | 74.05 | 83.15 | 70.47 | 86.05 | -0.58 | 2.95 | 85.73
| 051 | USIH_12A | 42.9 | 7.64 | 1350 | 1354 | 1352 | 1508 | 18+ | 31.63 | 32.23 | 32.63 | 27.65 | 56.77 | 0.10 | 5.66 | 56.40
| 052 | USIH_13A | 45.0 | 7.15 | 1426 | 1439 | 1435 | 1583 | 26 | 71.14 | 72.80 | 80.49 | 68.21 | 85.32 | -0.49 | 3.79 | 84.83
| 067 | USTH_01A | 48.9 | 6.38 | 1419 | 1425 | 1419 | 1570 | 26- | 53.82 | 55.15 | 58.98 | 49.98 | 74.26 | -0.60 | 4.90 | 73.79
| 068 | UST__02A | 39.7 | 7.11 | 1389 | 1399 | 1399 | 1554 | 20+ | 58.73 | 60.15 | 63.10 | 53.47 | 77.56 | -0.55 | 6.05 | 76.75
| 077 | USSH_01A | 51.2 | 6.56 | 1406 | 1411 | 1403 | 1557 | 26- | 53.65 | 54.91 | 58.86 | 49.88 | 74.10 | -0.44 | 4.78 | 73.66
| 078 | USSH_02A | 49.8 | 7.11 | 1407 | 1413 | 1406 | 1560 | 26- | 54.34 | 55.62 | 60.09 | 50.92 | 74.58 | -0.45 | 4.43 | 74.19
| 079 | USSH_03A | 49.5 | 6.60 | 1413 | 1420 | 1413 | 1566 | 26- | 53.98 | 55.23 | 59.76 | 50.64 | 74.32 | -0.40 | 4.35 | 73.95
| 055 | UKMH_02A | 50.4 | 8.20 | 1258 | 1266 | 1258 | 1391 | 13+ | 45.95 | 46.44 | 49.38 | 41.85 | 68.15 | 1.10 | 4.74 | 67.78
| 092 | KKSHP03A | 54.9 | 9.67 | 1428 | 1436 | 1425 | 1575 | 26 | 61.43 | 62.17 | 67.01 | 56.79 | 78.85 | 1.08 | 4.81 | 78.28
| 093 | KKSHP04S | 53.8 | 9.25 | 1409 | 1413 | 1403 | 1557 | 26- | 51.17 | 51.90 | 55.88 | 47.36 | 72.04 | 0.71 | 4.44 | 71.68
| 094 | KKSHP05A | 45.9 | 6.85 | 1312 | 1318 | 1314 | 1464 | 16+ | 47.35 | 47.58 | 49.93 | 42.31 | 68.98 | 1.82 | 5.37 | 68.46
| 095 | KKSHA06A | 49.4 | 7.08 | 1383 | 1390 | 1383 | 1539 | 20+ | 50.22 | 50.88 | 54.62 | 46.29 | 71.33 | 0.84 | 4.53 | 70.96
| 104 | KKSTH17A | 45.9 | 6.47 | 1331 | 1336 | 1332 | 1485 | 17+ | 52.31 | 52.92 | 55.33 | 46.89 | 72.75 | 1.05 | 5.83 | 72.11
| 134 | KHDHP01A | 47.3 | 9.54 | 1392 | 1405 | 1400 | 1554 | 20+ | 63.10 | 64.49 | 69.54 | 58.93 | 80.31 | -0.28 | 4.87 | 79.71
| 186 | MKKH_03A | 52.3 | 6.68 | 1391 | 1398 | 1389 | 1545 | 20+ | 50.57 | 51.91 | 54.91 | 46.53 | 72.05 | -0.80 | 5.25 | 71.55
| 057 | UMOH_01A | 49.8 | 6.64 | 1471 | 1482 | 1475 | 1610 | 27 | 75.05 | 76.76 | 87.47 | 74.13 | 87.61 | -0.42 | 2.14 | 87.42
| 157 | NMSH_03A | 49.0 | 9.47 | 1256 | 1274 | 1267 | 1404 | 14- | 36.77 | 36.26 | 39.46 | 33.44 | 60.22 | 3.62 | 3.30 | 59.92
| 159 | NMNH_01A | 47.6 | 4.98 | 1314 | 1315 | 1309 | 1459 | 16 | 50.18 | 50.74 | 54.49 | 46.18 | 71.23 | 1.09 | 4.51 | 70.86
| 161 | NMYH_03S | 48.7 | 6.86 | 1416 | 1422 | 1416 | 1568 | 26- | 44.79 | 45.77 | 49.45 | 41.91 | 67.65 | -0.22 | 4.02 | 67.40
| 164 | NMYTH02A | 48.6 | 7.83 | 1410 | 1416 | 1410 | 1563 | 26- | 50.54 | 51.76 | 55.15 | 46.74 | 71.94 | -0.51 | 4.91 | 71.51
| 165 | NMYH_04A | 50.0 | 7.14 | 1402 | 1406 | 1399 | 1553 | 20+ | 43.73 | 44.84 | 47.85 | 40.55 | 66.96 | -0.62 | 4.51 | 66.65
| 166 | NMYH_05A | 48.1 | 7.05 | 1452 | 1465 | 1459 | 1600 | 27- | 67.35 | 68.94 | 77.17 | 65.40 | 83.03 | -0.51 | 3.02 | 82.76
| 173 | HFIH_01S | 41.9 | 5.14 | 1582 | 1591 | 1590 | 1652 | 29 | 76.86 | 78.42 | 92.43 | 78.33 | 88.56 | -0.05 | 0.10 | 88.55
| 195 | SFDH_02A | 44.2 | 3.99 | 1561 | 1573 | 1570 | 1648 | 29 | 65.96 | 67.54 | 76.30 | 64.66 | 82.18 | -0.56 | 2.48 | 82.00
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