XRD, TGA and TMA Charts (No.068)
| No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
|---|---|---|---|---|---|---|---|
| 068 | UST__02A | March 30, 1982 | Sarayama V. | Toboshi | Ueda Tohseki | Right of USTH_01A | Look like Henshoku (discoloration) |
| Colors of the milled samples | |||||||
|---|---|---|---|---|---|---|---|
| X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
| 74.60 | 73.73 | 67.82 | 57.47 | 85.87 | 4.81 | 13.28 | 80.02 |
| Chemical compositions (wt%) | ||||||||
|---|---|---|---|---|---|---|---|---|
| SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
| 77.85 | 15.16 | 0.69 | 0.01 | 0.09 | 0.11 | 0.10 | 3.04 | 2.56 |
| Mineral compositions (wt%) | |||||
|---|---|---|---|---|---|
| Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
| 56.89 | 33.34 | 8.51 | 1.11 | 0.00 | 0.15 |
| Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 3.16 | 2.40 | 66.11 | 63.94 | 59.83 | 50.70 | 79.96 | 7.64 | 11.61 | 75.61
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| Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 39.7 | 7.11 | 1389 | 1399 | 1399 | 1554 | 20+ | 58.73 | 60.15 | 63.10 | 53.47 | 77.56 | -0.55 | 6.05 | 76.75
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