XRD, TGA and TMA Charts (No.198)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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198 | SFD__05A | March 26,1981 | Fukami V. | Fukami | Shin-ei Tohseki | Inside drift | White color, rough |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
86.33 | 86.68 | 95.61 | 81.03 | 93.10 | 2.59 | 4.28 | 91.48 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
78.78 | 15.34 | 0.16 | 0.04 | 0.06 | 0.10 | 0.05 | 0.43 | 4.57 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
57.98 | 0.01 | 41.34 | 0.55 | 0.01 | 0.11 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 5.33 | 4.41 | 85.26 | 86.17 | 93.46 | 79.20 | 92.83 | 1.50 | 5.29 | 90.97
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 44.6 | 4.82 | 1600 | 1600 | 1597 | 1653 | 29+ | 75.07 | 76.62 | 89.70 | 76.02 | 87.53 | -0.10 | 0.52 | 87.52
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