XRD, TGA and TMA Charts (No.107)

No.NameSampling dateVein or depositMining placeMining companySampling placeGrade or sort
107KGG4_03SMarch 26,1981Murayama V.GosohKiyama TohsekiIncline shaft working faceFourth grade, SK19, kaolin / sericite = 1

Colors of the milled samples
XYZWhiteness (Hunter)LabWhiteness (Lab)
60.9260.3449.9042.2977.684.0516.2972.07

Chemical compositions (wt%)
SiO2Al2O3Fe2O3TiO2CaOMgONa2OK2OIg.loss
75.2214.390.750.011.150.112.333.352.47


Mineral compositions (wt%)
Q : QuartzM : SericiteK : Kaolin mineralF : FeldsparC : CalciteS : Siderite
42.9722.188.8523.952.050.00


Results of TGA and Colors of the Powder Samples after Measuring
The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C.
LT (wt%)L400 (wt%)XYZWhiteness (Hunter)LabWhiteness (Lab)
2.852.2757.1753.0940.2934.1472.8612.5518.2264.99


Results of TMA and Colors of the Sintered Samples after Measuring
The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK.
W10
(wt%)
SMax
(%)
T0
(°C)
T5
(°C)
TS5
(°C)
TSK
(°C)
SKXYZW
(Hunter)
LabW
(Lab)
51.69.06125912691261139413+50.9551.0851.8643.9571.472.187.0170.54
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