XRD, TGA and TMA Charts (No.107)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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107 | KGG4_03S | March 26,1981 | Murayama V. | Gosoh | Kiyama Tohseki | Incline shaft working face | Fourth grade, SK19, kaolin / sericite = 1 |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
60.92 | 60.34 | 49.90 | 42.29 | 77.68 | 4.05 | 16.29 | 72.07 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
75.22 | 14.39 | 0.75 | 0.01 | 1.15 | 0.11 | 2.33 | 3.35 | 2.47 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
42.97 | 22.18 | 8.85 | 23.95 | 2.05 | 0.00 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 2.85 | 2.27 | 57.17 | 53.09 | 40.29 | 34.14 | 72.86 | 12.55 | 18.22 | 64.99
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 51.6 | 9.06 | 1259 | 1269 | 1261 | 1394 | 13+ | 50.95 | 51.08 | 51.86 | 43.95 | 71.47 | 2.18 | 7.01 | 70.54
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