XRD, TGA and TMA Charts (No.073)
| No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
|---|---|---|---|---|---|---|---|
| 073 | UST__07A | March 30, 1982 | Sarayama V. | Toboshi | Ueda Tohseki | Tip of Sarayama vein / right | ? |
| Colors of the milled samples | |||||||
|---|---|---|---|---|---|---|---|
| X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
| 73.12 | 72.08 | 59.09 | 50.08 | 84.90 | 5.16 | 18.16 | 75.82 |
| Chemical compositions (wt%) | ||||||||
|---|---|---|---|---|---|---|---|---|
| SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
| 78.40 | 14.75 | 0.76 | 0.01 | 0.05 | 0.08 | 0.08 | 2.90 | 2.71 |
| Mineral compositions (wt%) | |||||
|---|---|---|---|---|---|
| Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
| 56.42 | 30.31 | 12.61 | 0.60 | 0.00 | 0.06 |
| Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 3.16 | 2.53 | 65.09 | 60.91 | 49.16 | 41.66 | 78.04 | 12.29 | 17.28 | 69.47
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| Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 37.6 | 8.17 | 1418 | 1427 | 1429 | 1578 | 26 | 53.75 | 55.17 | 59.09 | 50.08 | 74.28 | -0.81 | 4.83 | 73.82
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