XRD, TGA and TMA Charts (No.018)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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018 | USGH_20A | November 13, 1982 | Sarayama V. | Gohtsu | Ueda Tohseki | ? | Shima-henshoku (stripes- discoloration) |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
73.67 | 73.32 | 61.88 | 52.44 | 85.63 | 3.73 | 17.09 | 77.36 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
74.55 | 15.25 | 0.77 | 0.01 | 1.25 | 0.12 | 1.97 | 2.15 | 3.42 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
43.01 | 25.51 | 13.18 | 16.03 | 2.20 | 0.07 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 4.14 | 3.21 | 65.54 | 62.02 | 50.11 | 42.47 | 78.75 | 10.73 | 17.40 | 70.51
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 46.5 | 7.32 | 1289 | 1298 | 1293 | 1438 | 15 | 58.89 | 59.59 | 60.77 | 51.50 | 77.19 | 1.08 | 7.36 | 76.01
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