XRD, TGA and TMA Charts (No.115)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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115 | KRT__08A | November 13,1982 | Tomioka D. | Tomioka | Kiyama Tohseki | Cliff beside road / left | Soft rock |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
70.80 | 70.36 | 58.27 | 49.38 | 83.88 | 3.87 | 17.53 | 75.87 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
73.74 | 15.58 | 1.25 | 0.10 | 0.09 | 0.43 | 2.35 | 3.56 | 2.43 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
44.03 | 22.61 | 5.20 | 27.92 | 0.00 | 0.24 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 3.14 | 2.20 | 59.93 | 55.52 | 40.28 | 34.14 | 74.51 | 13.17 | 20.11 | 64.96
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 39.5 | 5.94 | 1281 | 1298 | 1298 | 1445 | 15+ | 42.88 | 42.27 | 35.00 | 29.66 | 65.02 | 3.95 | 13.59 | 62.26
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