XRD, TGA and TMA Charts (No.031)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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031 | USDT_12A | July 16, 1980 | Sarayama V. | Denbeekoba | Ueda Tohseki | Stack | Low grade |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
74.55 | 75.28 | 64.48 | 54.64 | 86.76 | 1.53 | 16.67 | 78.66 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
76.82 | 15.48 | 0.66 | 0.01 | 0.09 | 0.14 | 0.72 | 3.16 | 2.42 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
55.87 | 27.63 | 11.36 | 5.10 | 0.00 | 0.04 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 3.15 | 2.23 | 70.39 | 68.02 | 55.13 | 46.72 | 82.47 | 8.02 | 18.10 | 73.56
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 48.2 | 6.69 | 1402 | 1412 | 1406 | 1560 | 26- | 60.26 | 61.68 | 66.24 | 56.14 | 78.54 | -0.48 | 4.97 | 77.96
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