XRD, TGA and TMA Charts (No.029)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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029 | USDT_10A | July 16, 1980 | Sarayama V. | Denbeekoba | Ueda Tohseki | Upper base / lower | Low grade |
Colors of the milled samples | |||||||
---|---|---|---|---|---|---|---|
X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
71.91 | 71.50 | 54.98 | 46.59 | 84.56 | 3.83 | 20.64 | 73.94 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
76.81 | 15.56 | 0.74 | 0.01 | 0.06 | 0.14 | 0.46 | 3.38 | 2.46 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
54.90 | 32.29 | 8.97 | 3.73 | 0.00 | 0.11 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 3.11 | 2.27 | 66.28 | 62.50 | 48.87 | 41.42 | 79.06 | 11.30 | 18.69 | 69.74
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 43.8 | 7.31 | 1393 | 1404 | 1401 | 1556 | 26- | 58.81 | 60.21 | 63.21 | 53.57 | 77.60 | -0.50 | 6.02 | 76.80
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