XRD, TGA and TMA Charts (No.027)
No. | Name | Sampling date | Vein or deposit | Mining place | Mining company | Sampling place | Grade or sort |
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027 | USDTA08A | March 29, 1980 | Sarayama V. | Denbeekoba | Ueda Tohseki | ? | Low grade; Albite (+) |
Colors of the milled samples | |||||||
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X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab) |
71.01 | 71.40 | 61.57 | 52.18 | 84.50 | 2.13 | 15.95 | 77.66 |
Chemical compositions (wt%) | ||||||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | TiO2 | CaO | MgO | Na2O | K2O | Ig.loss |
75.94 | 15.26 | 0.69 | 0.01 | 0.05 | 0.16 | 3.11 | 2.80 | 1.59 |
Mineral compositions (wt%) | |||||
---|---|---|---|---|---|
Q : Quartz | M : Sericite | K : Kaolin mineral | F : Feldspar | C : Calcite | S : Siderite |
40.54 | 31.04 | 2.01 | 26.35 | 0.00 | 0.06 |
Results of TGA and Colors of the Powder Samples after Measuring | |||||||||||||||||||||||||||||
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The conditions for TGA were sample weight : about 180mg, heating rate : 20°C/min, ended temperature : 1000°C.
LT : Total weight loss, L400 : Weight loss of 400-1000°C. LT (wt%) | L400 (wt%) | X | Y | Z | Whiteness (Hunter) | L | a | b | Whiteness (Lab)
| 2.23 | 1.41 | 67.44 | 64.56 | 51.98 | 44.05 | 80.35 | 9.21 | 17.89 | 71.88
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Results of TMA and Colors of the Sintered Samples after Measuring | ||||||||||||||||||||||||||||||||||||||||||||
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The conditions for TMA were compaction pressure : 250MPa, pellet diameter : 10mm, thickness : about 3mm, heating rate : 10°C/min, loading : 10g.
W10 : Contents of particles larger than 10µm, SMax : Maximum shrinkage, T0 : Temperature at the maximum shrinkage, T5 : Temperature at the expansion coefficient becomes 0.0005/°C, TS5 : Temperature rectified using the correlative equation, TSK : Nominal temperature equivalent to its SK. W10 | (wt%) SMax | (%) T0 | (°C) T5 | (°C) TS5 | (°C) TSK | (°C) SK | X | Y | Z | W | (Hunter) L | a | b | W | (Lab) 55.9 | 7.36 | 1284 | 1297 | 1285 | 1428 | 15- | 57.46 | 58.49 | 58.80 | 49.83 | 76.48 | 0.27 | 7.95 | 75.17
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